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Continuous flow photolysis of aryl azides: Preparation of 3H-azepinones

Photolysis of aryl azides to give nitrenes, and their subsequent rearrangement in the presence of water to give 3H-azepinones, is performed in continuous flow in a photoreactor constructed of fluorinated ethylene polymer (FEP) tubing. Fine tuning of the reaction conditions using the flow reactor all...

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Detalles Bibliográficos
Autores principales:	Bou-Hamdan, Farhan R, Lévesque, François, O'Brien, Alexander G, Seeberger, Peter H
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Beilstein-Institut 2011
Materias:	Letter
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3167900/ https://www.ncbi.nlm.nih.gov/pubmed/21915216 http://dx.doi.org/10.3762/bjoc.7.129

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