(2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate

The title compound, C(23)H(17)ClN(2)O(3)·C(2)H(6)O, is the stoichiometric 1:1 ethanol solvate of a racemic reaction product, which forms a conglomerate. The refined Flack parameter of 0.36 (3) indicates racemic twinning. In the structure, mol­ecules are linked into zigzag chains by a series of inter...

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Autores principales: Boughaleb, Adil, Zouihri, Hafid, Gmouh, Said, Kerbal, Abdelali, El yazidi, Mohamed
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200620/
https://www.ncbi.nlm.nih.gov/pubmed/22059010
http://dx.doi.org/10.1107/S1600536811032636
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author Boughaleb, Adil
Zouihri, Hafid
Gmouh, Said
Kerbal, Abdelali
El yazidi, Mohamed
author_facet Boughaleb, Adil
Zouihri, Hafid
Gmouh, Said
Kerbal, Abdelali
El yazidi, Mohamed
author_sort Boughaleb, Adil
collection PubMed
description The title compound, C(23)H(17)ClN(2)O(3)·C(2)H(6)O, is the stoichiometric 1:1 ethanol solvate of a racemic reaction product, which forms a conglomerate. The refined Flack parameter of 0.36 (3) indicates racemic twinning. In the structure, mol­ecules are linked into zigzag chains by a series of inter­molecular N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-32006202011-11-06 (2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate Boughaleb, Adil Zouihri, Hafid Gmouh, Said Kerbal, Abdelali El yazidi, Mohamed Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(23)H(17)ClN(2)O(3)·C(2)H(6)O, is the stoichiometric 1:1 ethanol solvate of a racemic reaction product, which forms a conglomerate. The refined Flack parameter of 0.36 (3) indicates racemic twinning. In the structure, mol­ecules are linked into zigzag chains by a series of inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2011-08-27 /pmc/articles/PMC3200620/ /pubmed/22059010 http://dx.doi.org/10.1107/S1600536811032636 Text en © Boughaleb et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Boughaleb, Adil
Zouihri, Hafid
Gmouh, Said
Kerbal, Abdelali
El yazidi, Mohamed
(2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate
title (2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate
title_full (2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate
title_fullStr (2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate
title_full_unstemmed (2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate
title_short (2RS,4′RS)-3′-(3-Chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′H-spiro­[indene-2,5′-isoxazol]-1(3H)-one ethanol monosolvate
title_sort (2rs,4′rs)-3′-(3-chloro-4-meth­oxy­phen­yl)-4′-phenyl-4′h-spiro­[indene-2,5′-isoxazol]-1(3h)-one ethanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200620/
https://www.ncbi.nlm.nih.gov/pubmed/22059010
http://dx.doi.org/10.1107/S1600536811032636
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