4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)

In the title compound, C(14)H(13)NO(4)S·0.5C(10)H(8)N(2), the two benzene rings are nearly perpendicular to each other [dihedral angle = 83.21 (10)°]. The bipyridine mol­ecule is centrosymmetric, the mid-point of the C—C bond linking the pyridine rings being located on an inversion center. Inter­mol...

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Autor principal: Huang, Miao-Ling
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200677/
https://www.ncbi.nlm.nih.gov/pubmed/22059045
http://dx.doi.org/10.1107/S1600536811034544
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author Huang, Miao-Ling
author_facet Huang, Miao-Ling
author_sort Huang, Miao-Ling
collection PubMed
description In the title compound, C(14)H(13)NO(4)S·0.5C(10)H(8)N(2), the two benzene rings are nearly perpendicular to each other [dihedral angle = 83.21 (10)°]. The bipyridine mol­ecule is centrosymmetric, the mid-point of the C—C bond linking the pyridine rings being located on an inversion center. Inter­molecular N—H⋯O and O—H⋯N hydrogen bonds and weak inter­molecular C—H⋯O hydrogen bonds are present in the crystal structure.
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spelling pubmed-32006772011-11-06 4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2) Huang, Miao-Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(13)NO(4)S·0.5C(10)H(8)N(2), the two benzene rings are nearly perpendicular to each other [dihedral angle = 83.21 (10)°]. The bipyridine mol­ecule is centrosymmetric, the mid-point of the C—C bond linking the pyridine rings being located on an inversion center. Inter­molecular N—H⋯O and O—H⋯N hydrogen bonds and weak inter­molecular C—H⋯O hydrogen bonds are present in the crystal structure. International Union of Crystallography 2011-08-27 /pmc/articles/PMC3200677/ /pubmed/22059045 http://dx.doi.org/10.1107/S1600536811034544 Text en © Miao-Ling Huang 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Huang, Miao-Ling
4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
title 4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
title_full 4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
title_fullStr 4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
title_full_unstemmed 4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
title_short 4,4′-Bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
title_sort 4,4′-bipyridine–4-(p-toluene­sulfonamido)­benzoic acid (1/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200677/
https://www.ncbi.nlm.nih.gov/pubmed/22059045
http://dx.doi.org/10.1107/S1600536811034544
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