2-Chloro-N-[2-(2-fluoro­benzo­yl)-4-nitro­phen­yl]-N-methyl­acetamide

The title compound, C(16)H(12)ClFN(2)O(4), crystallizes with two mol­ecules in the asymmetric unit in which the dihedral angles between the mean planes of the two benzene rings are 65.1 (7) and 65.6 (6)°. In each mol­ecule, the nitro group displays rotational disorder over two orientations in a 0.50...

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Detalles Bibliográficos
Autores principales: Siddaraju, B. P., Jasinski, Jerry P., Golen, James A., Yathirajan, H. S., Raju, C. R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200782/
https://www.ncbi.nlm.nih.gov/pubmed/22064922
http://dx.doi.org/10.1107/S1600536811034969
Descripción
Sumario:The title compound, C(16)H(12)ClFN(2)O(4), crystallizes with two mol­ecules in the asymmetric unit in which the dihedral angles between the mean planes of the two benzene rings are 65.1 (7) and 65.6 (6)°. In each mol­ecule, the nitro group displays rotational disorder over two orientations in a 0.503 (11):0.497 (11) ratio and the Cl atom is disordered in a 0.432 (5):0.568 (5) ratio. In one mol­ecule, the F atoms is statistically disordered over two positions. The crystal packing features weak inter­molecular C—H⋯O and C—H⋯Cl inter­actions, which form a layered network.

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