4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)

The asymmetric unit of the title compound C(20)H(30)N(4)S(2) (+). 2ClO(4) (−) comprises one macrocyclic cation and two perchlorate anions. In the cation, one of the protonated H atoms bound to the amide N atom is involved in an intra­molecular N—H⋯N hydrogen bond. The O atoms in the two perchlorate...

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Detalles Bibliográficos
Autores principales: Wei, ZhenHong, You, XiuLi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200833/
https://www.ncbi.nlm.nih.gov/pubmed/22058983
http://dx.doi.org/10.1107/S1600536811032715
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author Wei, ZhenHong
You, XiuLi
author_facet Wei, ZhenHong
You, XiuLi
author_sort Wei, ZhenHong
collection PubMed
description The asymmetric unit of the title compound C(20)H(30)N(4)S(2) (+). 2ClO(4) (−) comprises one macrocyclic cation and two perchlorate anions. In the cation, one of the protonated H atoms bound to the amide N atom is involved in an intra­molecular N—H⋯N hydrogen bond. The O atoms in the two perchlorate anions are disordered over two sets of sites with occupancy ratios of 0.65 (3):0.35 (3) and 0.640 (15):0.360 (15).
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spelling pubmed-32008332011-11-06 4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate) Wei, ZhenHong You, XiuLi Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound C(20)H(30)N(4)S(2) (+). 2ClO(4) (−) comprises one macrocyclic cation and two perchlorate anions. In the cation, one of the protonated H atoms bound to the amide N atom is involved in an intra­molecular N—H⋯N hydrogen bond. The O atoms in the two perchlorate anions are disordered over two sets of sites with occupancy ratios of 0.65 (3):0.35 (3) and 0.640 (15):0.360 (15). International Union of Crystallography 2011-08-27 /pmc/articles/PMC3200833/ /pubmed/22058983 http://dx.doi.org/10.1107/S1600536811032715 Text en © Wei and You 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wei, ZhenHong
You, XiuLi
4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
title 4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
title_full 4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
title_fullStr 4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
title_full_unstemmed 4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
title_short 4,10-Bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
title_sort 4,10-bis(pyridin-2-ylmeth­yl)-1,7-dithia-4,10-diazo­niacyclo­dodecane bis(perchlorate)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200833/
https://www.ncbi.nlm.nih.gov/pubmed/22058983
http://dx.doi.org/10.1107/S1600536811032715
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