Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate

In the structure of the title compound, C(17)H(18)ClN(3)O(4)S, the thia­zinane ring displays a twist-boat conformation. The 1,4-dihydro­pyridine ring is approximately perpendicular to the benzene ring [dihedral angle = 88.3 (1)°]. The mol­ecular conformation is stabilized by an intra­molecular N—H⋯O...

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Detalles Bibliográficos
Autores principales: Zhang, Na, Zhang, Xian, Li, Dongmei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200856/
https://www.ncbi.nlm.nih.gov/pubmed/22058968
http://dx.doi.org/10.1107/S1600536811032193
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author Zhang, Na
Zhang, Xian
Li, Dongmei
author_facet Zhang, Na
Zhang, Xian
Li, Dongmei
author_sort Zhang, Na
collection PubMed
description In the structure of the title compound, C(17)H(18)ClN(3)O(4)S, the thia­zinane ring displays a twist-boat conformation. The 1,4-dihydro­pyridine ring is approximately perpendicular to the benzene ring [dihedral angle = 88.3 (1)°]. The mol­ecular conformation is stabilized by an intra­molecular N—H⋯O hydrogen bond. In the crystal, mol­ecules are linked by N—H⋯O inter­actions into a C(8) chain along [100].
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spelling pubmed-32008562011-11-06 Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate Zhang, Na Zhang, Xian Li, Dongmei Acta Crystallogr Sect E Struct Rep Online Organic Papers In the structure of the title compound, C(17)H(18)ClN(3)O(4)S, the thia­zinane ring displays a twist-boat conformation. The 1,4-dihydro­pyridine ring is approximately perpendicular to the benzene ring [dihedral angle = 88.3 (1)°]. The mol­ecular conformation is stabilized by an intra­molecular N—H⋯O hydrogen bond. In the crystal, mol­ecules are linked by N—H⋯O inter­actions into a C(8) chain along [100]. International Union of Crystallography 2011-08-17 /pmc/articles/PMC3200856/ /pubmed/22058968 http://dx.doi.org/10.1107/S1600536811032193 Text en © Zhang et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Na
Zhang, Xian
Li, Dongmei
Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
title Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
title_full Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
title_fullStr Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
title_full_unstemmed Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
title_short Ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
title_sort ethyl 6-amino-8-(4-chloro­phen­yl)-9-nitro-2,3,4,8-tetra­hydro­pyrido[2,1-b][1,3]thia­zine-7-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200856/
https://www.ncbi.nlm.nih.gov/pubmed/22058968
http://dx.doi.org/10.1107/S1600536811032193
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AT zhangxian ethyl6amino84chlorophenyl9nitro2348tetrahydropyrido21b13thiazine7carboxylate
AT lidongmei ethyl6amino84chlorophenyl9nitro2348tetrahydropyrido21b13thiazine7carboxylate

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