1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate

In the title compound, C(72)H(80)N(2)·C(7)H(8), the acenaphthene ring system is essentially planar, with a maximum deviation of 0.041 (3) Å. The benzene rings bonded to the the N atoms are essentially parallel, forming a dihedral angle of 0.80 (11)°, and these rings form dihedral angles of 87.49 (9)...

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Detalles Bibliográficos
Autores principales: Lohr, Tracy L., Piers, Warren E., Parvez, Masood
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200865/
https://www.ncbi.nlm.nih.gov/pubmed/22058927
http://dx.doi.org/10.1107/S1600536811031242
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author Lohr, Tracy L.
Piers, Warren E.
Parvez, Masood
author_facet Lohr, Tracy L.
Piers, Warren E.
Parvez, Masood
author_sort Lohr, Tracy L.
collection PubMed
description In the title compound, C(72)H(80)N(2)·C(7)H(8), the acenaphthene ring system is essentially planar, with a maximum deviation of 0.041 (3) Å. The benzene rings bonded to the the N atoms are essentially parallel, forming a dihedral angle of 0.80 (11)°, and these rings form dihedral angles of 87.49 (9) and 88.25 (10)° with the mean plane of the acenaphthene ring system. The methyl C atoms of three of the isopropyl groups are disordered of two sets of sites of equal occupancy.
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spelling pubmed-32008652011-11-06 1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate Lohr, Tracy L. Piers, Warren E. Parvez, Masood Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(72)H(80)N(2)·C(7)H(8), the acenaphthene ring system is essentially planar, with a maximum deviation of 0.041 (3) Å. The benzene rings bonded to the the N atoms are essentially parallel, forming a dihedral angle of 0.80 (11)°, and these rings form dihedral angles of 87.49 (9) and 88.25 (10)° with the mean plane of the acenaphthene ring system. The methyl C atoms of three of the isopropyl groups are disordered of two sets of sites of equal occupancy. International Union of Crystallography 2011-08-11 /pmc/articles/PMC3200865/ /pubmed/22058927 http://dx.doi.org/10.1107/S1600536811031242 Text en © Lohr et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lohr, Tracy L.
Piers, Warren E.
Parvez, Masood
1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
title 1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
title_full 1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
title_fullStr 1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
title_full_unstemmed 1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
title_short 1,2-Bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
title_sort 1,2-bis{[3,5-bis­(2,6-diisopropyl­phen­yl)phen­yl]imino}­acenaphthene toluene monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200865/
https://www.ncbi.nlm.nih.gov/pubmed/22058927
http://dx.doi.org/10.1107/S1600536811031242
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AT pierswarrene 12bis35bis26diisopropylphenylphenyliminoacenaphthenetoluenemonosolvate
AT parvezmasood 12bis35bis26diisopropylphenylphenyliminoacenaphthenetoluenemonosolvate

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