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4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate
In the title compound, C(20)H(19)N(5)O(3)S·H(2)O, the pyrazole ring is connected to a pyrazolone ring, and the two five-membered rings are aligned at 45.0 (1)°. The pyrazole ring is connected to a phenyl ring and the two are twisted by 42.7 (1)°. Finally, the pyrazolone ring is connected to a benzen...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2011
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200878/ https://www.ncbi.nlm.nih.gov/pubmed/22059030 http://dx.doi.org/10.1107/S1600536811034453 |
| _version_ | 1782214769968676864 |
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| author | Asiri, Abdullah M. Al-Youbi, Abdulrahman O. Faidallah, Hassan M. Alamry, Khalid A. Ng, Seik Weng |
| author_facet | Asiri, Abdullah M. Al-Youbi, Abdulrahman O. Faidallah, Hassan M. Alamry, Khalid A. Ng, Seik Weng |
| author_sort | Asiri, Abdullah M. |
| collection | PubMed |
| description | In the title compound, C(20)H(19)N(5)O(3)S·H(2)O, the pyrazole ring is connected to a pyrazolone ring, and the two five-membered rings are aligned at 45.0 (1)°. The pyrazole ring is connected to a phenyl ring and the two are twisted by 42.7 (1)°. Finally, the pyrazolone ring is connected to a benzene ring and the two are twisted by 19.5 (1)°. The N—H and –NH(2) portions and the solvent water molecules are engaged in N—H⋯N, N—H⋯O and O—H⋯O hydrogen-bonding interactions to generate a three-dimensional network. |
| format | Online Article Text |
| id | pubmed-3200878 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2011 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-32008782011-11-06 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate Asiri, Abdullah M. Al-Youbi, Abdulrahman O. Faidallah, Hassan M. Alamry, Khalid A. Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(19)N(5)O(3)S·H(2)O, the pyrazole ring is connected to a pyrazolone ring, and the two five-membered rings are aligned at 45.0 (1)°. The pyrazole ring is connected to a phenyl ring and the two are twisted by 42.7 (1)°. Finally, the pyrazolone ring is connected to a benzene ring and the two are twisted by 19.5 (1)°. The N—H and –NH(2) portions and the solvent water molecules are engaged in N—H⋯N, N—H⋯O and O—H⋯O hydrogen-bonding interactions to generate a three-dimensional network. International Union of Crystallography 2011-08-27 /pmc/articles/PMC3200878/ /pubmed/22059030 http://dx.doi.org/10.1107/S1600536811034453 Text en © Asiri et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Asiri, Abdullah M. Al-Youbi, Abdulrahman O. Faidallah, Hassan M. Alamry, Khalid A. Ng, Seik Weng 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| title | 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| title_full | 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| title_fullStr | 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| title_full_unstemmed | 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| title_short | 4-(5,3′-Dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2H-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| title_sort | 4-(5,3′-dimethyl-5′-oxo-2-phenyl-2′,5′-dihydro-2h-[3,4′]bipyrazol-1′-yl)benzenesulfonamide monohydrate |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200878/ https://www.ncbi.nlm.nih.gov/pubmed/22059030 http://dx.doi.org/10.1107/S1600536811034453 |
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