rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one

The title racemic compound, C(13)H(18)O(3), a common precursor in the total synthesis of terpenes, crystallizes with two molecules in the asymmetric unit. The crystal structure is made up of triple chains, formed by weak inter­molecular C—H⋯O contacts, propagating in the a-axis direction.

Detalles Bibliográficos
Autores principales: Werner, Franz, Toon, Liina, Aav, Riina
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200915/
https://www.ncbi.nlm.nih.gov/pubmed/22064558
http://dx.doi.org/10.1107/S1600536811034349
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author Werner, Franz
Toon, Liina
Aav, Riina
author_facet Werner, Franz
Toon, Liina
Aav, Riina
author_sort Werner, Franz
collection PubMed
description The title racemic compound, C(13)H(18)O(3), a common precursor in the total synthesis of terpenes, crystallizes with two molecules in the asymmetric unit. The crystal structure is made up of triple chains, formed by weak inter­molecular C—H⋯O contacts, propagating in the a-axis direction.
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spelling pubmed-32009152011-11-06 rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one Werner, Franz Toon, Liina Aav, Riina Acta Crystallogr Sect E Struct Rep Online Organic Papers The title racemic compound, C(13)H(18)O(3), a common precursor in the total synthesis of terpenes, crystallizes with two molecules in the asymmetric unit. The crystal structure is made up of triple chains, formed by weak inter­molecular C—H⋯O contacts, propagating in the a-axis direction. International Union of Crystallography 2011-08-27 /pmc/articles/PMC3200915/ /pubmed/22064558 http://dx.doi.org/10.1107/S1600536811034349 Text en © Werner et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Werner, Franz
Toon, Liina
Aav, Riina
rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one
title rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one
title_full rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one
title_fullStr rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one
title_full_unstemmed rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one
title_short rac-8a’-Methyl-3′,4′,8′,8a’-tetra­hydro-2′H-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′H)-one
title_sort rac-8a’-methyl-3′,4′,8′,8a’-tetra­hydro-2′h-spiro­[[1,3]dioxolane-2,1′-naphthalen]-6′(7′h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3200915/
https://www.ncbi.nlm.nih.gov/pubmed/22064558
http://dx.doi.org/10.1107/S1600536811034349
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