(E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate

The title compound, C(9)H(10)N(2)O(3)·2H(2)O, crystallizes with two organic mol­ecules and four water mol­ecules in the asymmetric unit. Both organic mol­ecules adopt a trans conformation with respect to the C=N bond and are close to planar [dihedral angles between the side chain and the aromatic ri...

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Autores principales: Li, Wei-Wei, Yu, Tie-Ming, Lv, Lu-Ping, Hu, Xian-Chao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201241/
https://www.ncbi.nlm.nih.gov/pubmed/22058745
http://dx.doi.org/10.1107/S1600536811035689
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author Li, Wei-Wei
Yu, Tie-Ming
Lv, Lu-Ping
Hu, Xian-Chao
author_facet Li, Wei-Wei
Yu, Tie-Ming
Lv, Lu-Ping
Hu, Xian-Chao
author_sort Li, Wei-Wei
collection PubMed
description The title compound, C(9)H(10)N(2)O(3)·2H(2)O, crystallizes with two organic mol­ecules and four water mol­ecules in the asymmetric unit. Both organic mol­ecules adopt a trans conformation with respect to the C=N bond and are close to planar [dihedral angles between the side chain and the aromatic ring = 9.34 (8) and 4.96 (8)°]. In the crystal, the components are linked into three-dimensional network by N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-32012412011-11-06 (E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate Li, Wei-Wei Yu, Tie-Ming Lv, Lu-Ping Hu, Xian-Chao Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(9)H(10)N(2)O(3)·2H(2)O, crystallizes with two organic mol­ecules and four water mol­ecules in the asymmetric unit. Both organic mol­ecules adopt a trans conformation with respect to the C=N bond and are close to planar [dihedral angles between the side chain and the aromatic ring = 9.34 (8) and 4.96 (8)°]. In the crystal, the components are linked into three-dimensional network by N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2011-09-14 /pmc/articles/PMC3201241/ /pubmed/22058745 http://dx.doi.org/10.1107/S1600536811035689 Text en © Li et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Wei-Wei
Yu, Tie-Ming
Lv, Lu-Ping
Hu, Xian-Chao
(E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
title (E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
title_full (E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
title_fullStr (E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
title_full_unstemmed (E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
title_short (E)-Methyl N′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
title_sort (e)-methyl n′-(3-hy­droxy­benzyl­idene)hydrazinecarboxyl­ate dihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201241/
https://www.ncbi.nlm.nih.gov/pubmed/22058745
http://dx.doi.org/10.1107/S1600536811035689
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AT lvluping emethyln3hydroxybenzylidenehydrazinecarboxylatedihydrate
AT huxianchao emethyln3hydroxybenzylidenehydrazinecarboxylatedihydrate

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