N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide

In the title compound, C(14)H(10)I(2)N(2)O(2), the two aromatic rings are inclined at a dihedral angle of 16.72 (33)°. The mol­ecular structure is stabilized by an intra­molecular O—H⋯N hydrogen bond. In the crystal, inter­molecular N—H⋯O inter­actions link the mol­ecules into chains running along t...

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Autores principales: Thirugnanasundar, A., Suresh, J., Meenakshi, C., Chakkaravarthi, G., Rajagopal, G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201245/
https://www.ncbi.nlm.nih.gov/pubmed/22064780
http://dx.doi.org/10.1107/S1600536811036488
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author Thirugnanasundar, A.
Suresh, J.
Meenakshi, C.
Chakkaravarthi, G.
Rajagopal, G.
author_facet Thirugnanasundar, A.
Suresh, J.
Meenakshi, C.
Chakkaravarthi, G.
Rajagopal, G.
author_sort Thirugnanasundar, A.
collection PubMed
description In the title compound, C(14)H(10)I(2)N(2)O(2), the two aromatic rings are inclined at a dihedral angle of 16.72 (33)°. The mol­ecular structure is stabilized by an intra­molecular O—H⋯N hydrogen bond. In the crystal, inter­molecular N—H⋯O inter­actions link the mol­ecules into chains running along the c axis. C—H⋯O inter­actions also occur. The crystal used for the structure determination was a non-merohedral twin with a domain ratio of 0.972 (2):0.028 (2).
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spelling pubmed-32012452011-11-06 N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide Thirugnanasundar, A. Suresh, J. Meenakshi, C. Chakkaravarthi, G. Rajagopal, G. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(10)I(2)N(2)O(2), the two aromatic rings are inclined at a dihedral angle of 16.72 (33)°. The mol­ecular structure is stabilized by an intra­molecular O—H⋯N hydrogen bond. In the crystal, inter­molecular N—H⋯O inter­actions link the mol­ecules into chains running along the c axis. C—H⋯O inter­actions also occur. The crystal used for the structure determination was a non-merohedral twin with a domain ratio of 0.972 (2):0.028 (2). International Union of Crystallography 2011-09-14 /pmc/articles/PMC3201245/ /pubmed/22064780 http://dx.doi.org/10.1107/S1600536811036488 Text en © Thirugnanasundar et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Thirugnanasundar, A.
Suresh, J.
Meenakshi, C.
Chakkaravarthi, G.
Rajagopal, G.
N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
title N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
title_full N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
title_fullStr N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
title_full_unstemmed N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
title_short N′-[(E)-2-Hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
title_sort n′-[(e)-2-hy­droxy-3,5-diiodo­benzyl­idene]cyclo­hexa­ne-1-carbohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201245/
https://www.ncbi.nlm.nih.gov/pubmed/22064780
http://dx.doi.org/10.1107/S1600536811036488
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