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(E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate

In the title compound, C(12)H(12)N(2)O(3)S·2C(2)H(6)OS, the acetic acid and cinnamoyl groups adopt Z and E configurations, respectively, with respect to the thio group about the C—N bonds. The components of the asymmetric unit are connected by N—H⋯O and O—H⋯O hydrogen bonds and in the crystal weak i...

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Autores principales: Hassan, Ibrahim N., Wan Daud, Wan Ramli, Yamin, Bohari M., Kassim, Mohammad B.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201284/
https://www.ncbi.nlm.nih.gov/pubmed/22058788
http://dx.doi.org/10.1107/S1600536811036750
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author Hassan, Ibrahim N.
Wan Daud, Wan Ramli
Yamin, Bohari M.
Kassim, Mohammad B.
author_facet Hassan, Ibrahim N.
Wan Daud, Wan Ramli
Yamin, Bohari M.
Kassim, Mohammad B.
author_sort Hassan, Ibrahim N.
collection PubMed
description In the title compound, C(12)H(12)N(2)O(3)S·2C(2)H(6)OS, the acetic acid and cinnamoyl groups adopt Z and E configurations, respectively, with respect to the thio group about the C—N bonds. The components of the asymmetric unit are connected by N—H⋯O and O—H⋯O hydrogen bonds and in the crystal weak inter­molecular C—H⋯O and C—H⋯S hydrogen bonds further connect the components into chains along the b axis. In the main mol­ecule, an intra­molecular N—H⋯O hydrogen bond is also present.
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spelling pubmed-32012842011-11-06 (E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate Hassan, Ibrahim N. Wan Daud, Wan Ramli Yamin, Bohari M. Kassim, Mohammad B. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(12)H(12)N(2)O(3)S·2C(2)H(6)OS, the acetic acid and cinnamoyl groups adopt Z and E configurations, respectively, with respect to the thio group about the C—N bonds. The components of the asymmetric unit are connected by N—H⋯O and O—H⋯O hydrogen bonds and in the crystal weak inter­molecular C—H⋯O and C—H⋯S hydrogen bonds further connect the components into chains along the b axis. In the main mol­ecule, an intra­molecular N—H⋯O hydrogen bond is also present. International Union of Crystallography 2011-09-17 /pmc/articles/PMC3201284/ /pubmed/22058788 http://dx.doi.org/10.1107/S1600536811036750 Text en © Hassan et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hassan, Ibrahim N.
Wan Daud, Wan Ramli
Yamin, Bohari M.
Kassim, Mohammad B.
(E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
title (E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
title_full (E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
title_fullStr (E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
title_full_unstemmed (E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
title_short (E)-2-(3-Cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
title_sort (e)-2-(3-cinnamoyl­thio­ureido)acetic acid dimethyl sulfoxide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201284/
https://www.ncbi.nlm.nih.gov/pubmed/22058788
http://dx.doi.org/10.1107/S1600536811036750
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