tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate

In the crystal structure of the title compound, C(22)H(25)NO(4), inter­molecular O—H⋯O hydrogen bonds involving the hy­droxy group of the 4-(amimometh­yl)phenol fragment and the C=O group connect the mol­ecules into infinite chains along the c axis. Two C atoms of the propyne group are disordered ov...

Descripción completa

Detalles Bibliográficos
Autores principales: Ao, Lei, Tu, Jie-Hong, Huang, Xuan, Ding, Bao-Yue
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201299/
https://www.ncbi.nlm.nih.gov/pubmed/22058772
http://dx.doi.org/10.1107/S160053681103683X
_version_ 1782214842605633536
author Ao, Lei
Tu, Jie-Hong
Huang, Xuan
Ding, Bao-Yue
author_facet Ao, Lei
Tu, Jie-Hong
Huang, Xuan
Ding, Bao-Yue
author_sort Ao, Lei
collection PubMed
description In the crystal structure of the title compound, C(22)H(25)NO(4), inter­molecular O—H⋯O hydrogen bonds involving the hy­droxy group of the 4-(amimometh­yl)phenol fragment and the C=O group connect the mol­ecules into infinite chains along the c axis. Two C atoms of the propyne group are disordered over two sites with occupancy factors of 0.53 (2) and 0.47 (2).
format Online
Article
Text
id pubmed-3201299
institution National Center for Biotechnology Information
language English
publishDate 2011
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32012992011-11-06 tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate Ao, Lei Tu, Jie-Hong Huang, Xuan Ding, Bao-Yue Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(22)H(25)NO(4), inter­molecular O—H⋯O hydrogen bonds involving the hy­droxy group of the 4-(amimometh­yl)phenol fragment and the C=O group connect the mol­ecules into infinite chains along the c axis. Two C atoms of the propyne group are disordered over two sites with occupancy factors of 0.53 (2) and 0.47 (2). International Union of Crystallography 2011-09-14 /pmc/articles/PMC3201299/ /pubmed/22058772 http://dx.doi.org/10.1107/S160053681103683X Text en © Ao et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ao, Lei
Tu, Jie-Hong
Huang, Xuan
Ding, Bao-Yue
tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate
title tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate
title_full tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate
title_fullStr tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate
title_full_unstemmed tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate
title_short tert-Butyl N-(4-hy­droxy­benz­yl)-N-[4-(prop-2-yn­yloxy)benz­yl]carbamate
title_sort tert-butyl n-(4-hy­droxy­benz­yl)-n-[4-(prop-2-yn­yloxy)benz­yl]carbamate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201299/
https://www.ncbi.nlm.nih.gov/pubmed/22058772
http://dx.doi.org/10.1107/S160053681103683X
work_keys_str_mv AT aolei tertbutyln4hydroxybenzyln4prop2ynyloxybenzylcarbamate
AT tujiehong tertbutyln4hydroxybenzyln4prop2ynyloxybenzylcarbamate
AT huangxuan tertbutyln4hydroxybenzyln4prop2ynyloxybenzylcarbamate
AT dingbaoyue tertbutyln4hydroxybenzyln4prop2ynyloxybenzylcarbamate

Ejemplares similares