5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide

In the title compound C(11)H(13)N(3)OS, the aromatic ring and the dihydro­pyrazole ring are oriented orthogonally with respect to each other, making a dihedral angle of 89.92 (9)°. An intra­molecular O—H⋯S hydrogen bond occurs. In the crystal, weak N—H⋯N and N—H⋯S hydrogen bonds link the mol­ecules...

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Detalles Bibliográficos
Autores principales: Ganguly, Biplab, Foi, Ana, Doctorovich, Fabio, K. Dey, Benu, G. Roy, Tapashi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201317/
https://www.ncbi.nlm.nih.gov/pubmed/22065480
http://dx.doi.org/10.1107/S1600536811036658
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author Ganguly, Biplab
Foi, Ana
Doctorovich, Fabio
K. Dey, Benu
G. Roy, Tapashi
author_facet Ganguly, Biplab
Foi, Ana
Doctorovich, Fabio
K. Dey, Benu
G. Roy, Tapashi
author_sort Ganguly, Biplab
collection PubMed
description In the title compound C(11)H(13)N(3)OS, the aromatic ring and the dihydro­pyrazole ring are oriented orthogonally with respect to each other, making a dihedral angle of 89.92 (9)°. An intra­molecular O—H⋯S hydrogen bond occurs. In the crystal, weak N—H⋯N and N—H⋯S hydrogen bonds link the mol­ecules into a columnar stack propagating along the b axis.
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spelling pubmed-32013172011-11-06 5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide Ganguly, Biplab Foi, Ana Doctorovich, Fabio K. Dey, Benu G. Roy, Tapashi Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound C(11)H(13)N(3)OS, the aromatic ring and the dihydro­pyrazole ring are oriented orthogonally with respect to each other, making a dihedral angle of 89.92 (9)°. An intra­molecular O—H⋯S hydrogen bond occurs. In the crystal, weak N—H⋯N and N—H⋯S hydrogen bonds link the mol­ecules into a columnar stack propagating along the b axis. International Union of Crystallography 2011-09-30 /pmc/articles/PMC3201317/ /pubmed/22065480 http://dx.doi.org/10.1107/S1600536811036658 Text en © Ganguly et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ganguly, Biplab
Foi, Ana
Doctorovich, Fabio
K. Dey, Benu
G. Roy, Tapashi
5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide
title 5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide
title_full 5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide
title_fullStr 5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide
title_full_unstemmed 5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide
title_short 5-Hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1H-pyrazole-1-carbothio­amide
title_sort 5-hy­droxy-3-methyl-5-phenyl-4,5-di­hydro-1h-pyrazole-1-carbothio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201317/
https://www.ncbi.nlm.nih.gov/pubmed/22065480
http://dx.doi.org/10.1107/S1600536811036658
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