4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)

In the title 1/2 adduct, C(10)H(8)N(2)·2C(7)H(6)O(2)S, the dihedral angle between the pyridine rings is 18.41 (11)°. In the thio­phene­acrylic acid mol­ecules, the dihedral angles between the respective thio­phene and acrylic acid units are 5.52 (17)° and 23.92 (9)°. In the crystal, the components a...

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Autores principales: Rajakannu, Palanisamy, Hussain, Firasat, Sathiyendiran, Malaichamy
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201325/
https://www.ncbi.nlm.nih.gov/pubmed/22065617
http://dx.doi.org/10.1107/S1600536811035823
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author Rajakannu, Palanisamy
Hussain, Firasat
Sathiyendiran, Malaichamy
author_facet Rajakannu, Palanisamy
Hussain, Firasat
Sathiyendiran, Malaichamy
author_sort Rajakannu, Palanisamy
collection PubMed
description In the title 1/2 adduct, C(10)H(8)N(2)·2C(7)H(6)O(2)S, the dihedral angle between the pyridine rings is 18.41 (11)°. In the thio­phene­acrylic acid mol­ecules, the dihedral angles between the respective thio­phene and acrylic acid units are 5.52 (17)° and 23.92 (9)°. In the crystal, the components are linked via O—H⋯N hydrogen-bonding inter­actions, forming units of two 3-thio­phene­acrylic acid mol­ecules and one 4,4′-bipyridine mol­ecule.
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spelling pubmed-32013252011-11-06 4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2) Rajakannu, Palanisamy Hussain, Firasat Sathiyendiran, Malaichamy Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title 1/2 adduct, C(10)H(8)N(2)·2C(7)H(6)O(2)S, the dihedral angle between the pyridine rings is 18.41 (11)°. In the thio­phene­acrylic acid mol­ecules, the dihedral angles between the respective thio­phene and acrylic acid units are 5.52 (17)° and 23.92 (9)°. In the crystal, the components are linked via O—H⋯N hydrogen-bonding inter­actions, forming units of two 3-thio­phene­acrylic acid mol­ecules and one 4,4′-bipyridine mol­ecule. International Union of Crystallography 2011-09-14 /pmc/articles/PMC3201325/ /pubmed/22065617 http://dx.doi.org/10.1107/S1600536811035823 Text en © Rajakannu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rajakannu, Palanisamy
Hussain, Firasat
Sathiyendiran, Malaichamy
4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
title 4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
title_full 4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
title_fullStr 4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
title_full_unstemmed 4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
title_short 4,4′-Bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
title_sort 4,4′-bipyridine–3-(thio­phen-3-yl)acrylic acid (1/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201325/
https://www.ncbi.nlm.nih.gov/pubmed/22065617
http://dx.doi.org/10.1107/S1600536811035823
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