3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile

In the title compound, C(22)H(14)BrN(3), the fused-ring system is buckled owing to the ethyl­ene linkage in the central ring; the two flanking aromatic rings are twisted by 25.9 (1) ° with respect to each other. The phenyl ring is twisted by 77.0 (1)° relative to the amino- and cyano-bearing aromati...

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Autores principales: Asiri, Abdullah M., Faidallah, Hassan M., Al-Youbi, Abdulrahman O., Ng, Seik Weng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201339/
https://www.ncbi.nlm.nih.gov/pubmed/22058805
http://dx.doi.org/10.1107/S1600536811038517
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author Asiri, Abdullah M.
Faidallah, Hassan M.
Al-Youbi, Abdulrahman O.
Ng, Seik Weng
author_facet Asiri, Abdullah M.
Faidallah, Hassan M.
Al-Youbi, Abdulrahman O.
Ng, Seik Weng
author_sort Asiri, Abdullah M.
collection PubMed
description In the title compound, C(22)H(14)BrN(3), the fused-ring system is buckled owing to the ethyl­ene linkage in the central ring; the two flanking aromatic rings are twisted by 25.9 (1) ° with respect to each other. The phenyl ring is twisted by 77.0 (1)° relative to the amino- and cyano-bearing aromatic ring. In the crystal, adjacent mol­ecules are linked by two N–H⋯N hydrogen bonds, generating a zigzag chain along [101].
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spelling pubmed-32013392011-11-06 3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile Asiri, Abdullah M. Faidallah, Hassan M. Al-Youbi, Abdulrahman O. Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(22)H(14)BrN(3), the fused-ring system is buckled owing to the ethyl­ene linkage in the central ring; the two flanking aromatic rings are twisted by 25.9 (1) ° with respect to each other. The phenyl ring is twisted by 77.0 (1)° relative to the amino- and cyano-bearing aromatic ring. In the crystal, adjacent mol­ecules are linked by two N–H⋯N hydrogen bonds, generating a zigzag chain along [101]. International Union of Crystallography 2011-09-30 /pmc/articles/PMC3201339/ /pubmed/22058805 http://dx.doi.org/10.1107/S1600536811038517 Text en © Asiri et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Asiri, Abdullah M.
Faidallah, Hassan M.
Al-Youbi, Abdulrahman O.
Ng, Seik Weng
3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
title 3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
title_full 3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
title_fullStr 3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
title_full_unstemmed 3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
title_short 3-Amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
title_sort 3-amino-1-(4-bromo­phen­yl)-9,10-dihydro­phenanthrene-2,4-dicarbonitrile
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201339/
https://www.ncbi.nlm.nih.gov/pubmed/22058805
http://dx.doi.org/10.1107/S1600536811038517
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