(Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one

The mol­ecule of the title compound, C(23)H(20)N(4)O, assumes a non-planar conformation in which the pyrazolone ring forms dihedral angles of 10.33 (11), 65.34 (11) and 63.52 (10)° with the three benzene rings. In the crystal, the mol­ecules are linked by inter­molecular N—H⋯N hydrogen bonds, genera...

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Detalles Bibliográficos
Autores principales: Lu, Rong, Xia, Hua, Lü, Xingqiang, Zhao, Shunsheng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201420/
https://www.ncbi.nlm.nih.gov/pubmed/22065632
http://dx.doi.org/10.1107/S1600536811037470
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author Lu, Rong
Xia, Hua
Lü, Xingqiang
Zhao, Shunsheng
author_facet Lu, Rong
Xia, Hua
Lü, Xingqiang
Zhao, Shunsheng
author_sort Lu, Rong
collection PubMed
description The mol­ecule of the title compound, C(23)H(20)N(4)O, assumes a non-planar conformation in which the pyrazolone ring forms dihedral angles of 10.33 (11), 65.34 (11) and 63.52 (10)° with the three benzene rings. In the crystal, the mol­ecules are linked by inter­molecular N—H⋯N hydrogen bonds, generating chains parallel to the b axis. The secondary amino group is involved in an intra­molecular N—H⋯O hydrogen bond.
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spelling pubmed-32014202011-11-06 (Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one Lu, Rong Xia, Hua Lü, Xingqiang Zhao, Shunsheng Acta Crystallogr Sect E Struct Rep Online Organic Papers The mol­ecule of the title compound, C(23)H(20)N(4)O, assumes a non-planar conformation in which the pyrazolone ring forms dihedral angles of 10.33 (11), 65.34 (11) and 63.52 (10)° with the three benzene rings. In the crystal, the mol­ecules are linked by inter­molecular N—H⋯N hydrogen bonds, generating chains parallel to the b axis. The secondary amino group is involved in an intra­molecular N—H⋯O hydrogen bond. International Union of Crystallography 2011-09-30 /pmc/articles/PMC3201420/ /pubmed/22065632 http://dx.doi.org/10.1107/S1600536811037470 Text en © Lu et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lu, Rong
Xia, Hua
Lü, Xingqiang
Zhao, Shunsheng
(Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
title (Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
title_full (Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
title_fullStr (Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
title_full_unstemmed (Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
title_short (Z)-4-[(2-Amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
title_sort (z)-4-[(2-amino­anilino)(phen­yl)methyl­idene]-3-methyl-1-phenyl-1h-pyrazol-5(4h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201420/
https://www.ncbi.nlm.nih.gov/pubmed/22065632
http://dx.doi.org/10.1107/S1600536811037470
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