4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide

In the title mol­ecule, C(12)H(13)N(5)O(2)S, a bifurcated intra­molecular N—H⋯O(O) hydrogen bond forms two S(6) ring motifs. The benzene ring forms a dihedral angle of 14.36 (11)° with the pyrazole ring. In the crystal, pairs of N—H⋯S hydrogen bonds form centrosymmetric dimers, generating R (2) (2)(...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Arshad, Suhana, Shetty, Shobhitha, Kalluraya, Balakrishna
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201502/
https://www.ncbi.nlm.nih.gov/pubmed/22065021
http://dx.doi.org/10.1107/S1600536811037883
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author Fun, Hoong-Kun
Arshad, Suhana
Shetty, Shobhitha
Kalluraya, Balakrishna
author_facet Fun, Hoong-Kun
Arshad, Suhana
Shetty, Shobhitha
Kalluraya, Balakrishna
author_sort Fun, Hoong-Kun
collection PubMed
description In the title mol­ecule, C(12)H(13)N(5)O(2)S, a bifurcated intra­molecular N—H⋯O(O) hydrogen bond forms two S(6) ring motifs. The benzene ring forms a dihedral angle of 14.36 (11)° with the pyrazole ring. In the crystal, pairs of N—H⋯S hydrogen bonds form centrosymmetric dimers, generating R (2) (2)(8) ring motifs, which stack along the b axis.
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spelling pubmed-32015022011-11-06 4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide Fun, Hoong-Kun Arshad, Suhana Shetty, Shobhitha Kalluraya, Balakrishna Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(12)H(13)N(5)O(2)S, a bifurcated intra­molecular N—H⋯O(O) hydrogen bond forms two S(6) ring motifs. The benzene ring forms a dihedral angle of 14.36 (11)° with the pyrazole ring. In the crystal, pairs of N—H⋯S hydrogen bonds form centrosymmetric dimers, generating R (2) (2)(8) ring motifs, which stack along the b axis. International Union of Crystallography 2011-09-30 /pmc/articles/PMC3201502/ /pubmed/22065021 http://dx.doi.org/10.1107/S1600536811037883 Text en © Fun et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Arshad, Suhana
Shetty, Shobhitha
Kalluraya, Balakrishna
4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title 4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_full 4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_fullStr 4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_full_unstemmed 4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_short 4-[2-(2-Meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_sort 4-[2-(2-meth­oxy­phen­yl)hydrazinyl­idene]-3-methyl-5-oxo-4,5-dihydro-1h-pyrazole-1-carbothio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201502/
https://www.ncbi.nlm.nih.gov/pubmed/22065021
http://dx.doi.org/10.1107/S1600536811037883
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