7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one

The title compound, C(10)H(9)F(3)N(2)O(2), was prepared by the reaction of m-phenyl­enediamine and ethyl 4,4,4-trifluoro­acetoacetate. In the crystal, inter­molecular C—H⋯ F, N—H⋯F, O—H⋯N and N—H⋯O inter­actions contribute to the crystal packing.

Detalles Bibliográficos
Autores principales: Qin, Yuan, Xi, Haitao, Chen, Liang, Sun, Xiaoqiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201506/
https://www.ncbi.nlm.nih.gov/pubmed/22058761
http://dx.doi.org/10.1107/S1600536811035471
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author Qin, Yuan
Xi, Haitao
Chen, Liang
Sun, Xiaoqiang
author_facet Qin, Yuan
Xi, Haitao
Chen, Liang
Sun, Xiaoqiang
author_sort Qin, Yuan
collection PubMed
description The title compound, C(10)H(9)F(3)N(2)O(2), was prepared by the reaction of m-phenyl­enediamine and ethyl 4,4,4-trifluoro­acetoacetate. In the crystal, inter­molecular C—H⋯ F, N—H⋯F, O—H⋯N and N—H⋯O inter­actions contribute to the crystal packing.
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spelling pubmed-32015062011-11-06 7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one Qin, Yuan Xi, Haitao Chen, Liang Sun, Xiaoqiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(9)F(3)N(2)O(2), was prepared by the reaction of m-phenyl­enediamine and ethyl 4,4,4-trifluoro­acetoacetate. In the crystal, inter­molecular C—H⋯ F, N—H⋯F, O—H⋯N and N—H⋯O inter­actions contribute to the crystal packing. International Union of Crystallography 2011-09-14 /pmc/articles/PMC3201506/ /pubmed/22058761 http://dx.doi.org/10.1107/S1600536811035471 Text en © Qin et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Qin, Yuan
Xi, Haitao
Chen, Liang
Sun, Xiaoqiang
7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one
title 7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one
title_full 7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one
title_fullStr 7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one
title_full_unstemmed 7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one
title_short 7-Amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1H)-one
title_sort 7-amino-4-hy­droxy-4-trifluoro­methyl-3,4-dihydro­quinolin-2(1h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201506/
https://www.ncbi.nlm.nih.gov/pubmed/22058761
http://dx.doi.org/10.1107/S1600536811035471
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AT xihaitao 7amino4hydroxy4trifluoromethyl34dihydroquinolin21hone
AT chenliang 7amino4hydroxy4trifluoromethyl34dihydroquinolin21hone
AT sunxiaoqiang 7amino4hydroxy4trifluoromethyl34dihydroquinolin21hone

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