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Formation of SiC nanoparticles in an atmospheric microwave plasma
We describe the formation of SiC nanopowder using an atmospheric argon microwave plasma with tetramethylsilane (TMS) as precursor. The impact of several process conditions on the particle size of the product is experimentally investigated. Particles with sizes ranging from 7 nm to about 20 nm accord...
Autores principales: | , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Beilstein-Institut
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201619/ https://www.ncbi.nlm.nih.gov/pubmed/22043455 http://dx.doi.org/10.3762/bjnano.2.71 |
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author | Vennekamp, Martin Bauer, Ingolf Groh, Matthias Sperling, Evgeni Ueberlein, Susanne Myndyk, Maksym Mäder, Gerrit Kaskel, Stefan |
author_facet | Vennekamp, Martin Bauer, Ingolf Groh, Matthias Sperling, Evgeni Ueberlein, Susanne Myndyk, Maksym Mäder, Gerrit Kaskel, Stefan |
author_sort | Vennekamp, Martin |
collection | PubMed |
description | We describe the formation of SiC nanopowder using an atmospheric argon microwave plasma with tetramethylsilane (TMS) as precursor. The impact of several process conditions on the particle size of the product is experimentally investigated. Particles with sizes ranging from 7 nm to about 20 nm according to BET and XRD measurements are produced. The dependency of the particle size on the process parameters is evaluated statistically and explained with growth-rate equations derived from the theory of Ostwald ripening. The results show that the particle size is mainly influenced by the concentration of the precursor material in the plasma. |
format | Online Article Text |
id | pubmed-3201619 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | Beilstein-Institut |
record_format | MEDLINE/PubMed |
spelling | pubmed-32016192011-10-31 Formation of SiC nanoparticles in an atmospheric microwave plasma Vennekamp, Martin Bauer, Ingolf Groh, Matthias Sperling, Evgeni Ueberlein, Susanne Myndyk, Maksym Mäder, Gerrit Kaskel, Stefan Beilstein J Nanotechnol Full Research Paper We describe the formation of SiC nanopowder using an atmospheric argon microwave plasma with tetramethylsilane (TMS) as precursor. The impact of several process conditions on the particle size of the product is experimentally investigated. Particles with sizes ranging from 7 nm to about 20 nm according to BET and XRD measurements are produced. The dependency of the particle size on the process parameters is evaluated statistically and explained with growth-rate equations derived from the theory of Ostwald ripening. The results show that the particle size is mainly influenced by the concentration of the precursor material in the plasma. Beilstein-Institut 2011-10-07 /pmc/articles/PMC3201619/ /pubmed/22043455 http://dx.doi.org/10.3762/bjnano.2.71 Text en Copyright © 2011, Vennekamp et al. https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjnano/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Nanotechnology terms and conditions: (https://www.beilstein-journals.org/bjnano/terms) |
spellingShingle | Full Research Paper Vennekamp, Martin Bauer, Ingolf Groh, Matthias Sperling, Evgeni Ueberlein, Susanne Myndyk, Maksym Mäder, Gerrit Kaskel, Stefan Formation of SiC nanoparticles in an atmospheric microwave plasma |
title | Formation of SiC nanoparticles in an atmospheric microwave plasma |
title_full | Formation of SiC nanoparticles in an atmospheric microwave plasma |
title_fullStr | Formation of SiC nanoparticles in an atmospheric microwave plasma |
title_full_unstemmed | Formation of SiC nanoparticles in an atmospheric microwave plasma |
title_short | Formation of SiC nanoparticles in an atmospheric microwave plasma |
title_sort | formation of sic nanoparticles in an atmospheric microwave plasma |
topic | Full Research Paper |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3201619/ https://www.ncbi.nlm.nih.gov/pubmed/22043455 http://dx.doi.org/10.3762/bjnano.2.71 |
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