5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)

The title compound, C(19)H(18)Cl(2)O(8), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 2,4-dichloro­benzaldehyde in ethanol. The two 1,3-dioxane rings exhibit boat conformations. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O and C—H⋯Cl hydrogen bonds, f...

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Detalles Bibliográficos
Autor principal: Zeng, Wu-Lan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3212288/
https://www.ncbi.nlm.nih.gov/pubmed/22090945
http://dx.doi.org/10.1107/S1600536811025384
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author Zeng, Wu-Lan
author_facet Zeng, Wu-Lan
author_sort Zeng, Wu-Lan
collection PubMed
description The title compound, C(19)H(18)Cl(2)O(8), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 2,4-dichloro­benzaldehyde in ethanol. The two 1,3-dioxane rings exhibit boat conformations. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O and C—H⋯Cl hydrogen bonds, forming chains parallel to the a axis.
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spelling pubmed-32122882011-11-16 5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione) Zeng, Wu-Lan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(18)Cl(2)O(8), was prepared by the reaction of 2,2-dimethyl-1,3-dioxane-4,6-dione and 2,4-dichloro­benzaldehyde in ethanol. The two 1,3-dioxane rings exhibit boat conformations. In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O and C—H⋯Cl hydrogen bonds, forming chains parallel to the a axis. International Union of Crystallography 2011-07-02 /pmc/articles/PMC3212288/ /pubmed/22090945 http://dx.doi.org/10.1107/S1600536811025384 Text en © Wu-Lan Zeng 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zeng, Wu-Lan
5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
title 5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
title_full 5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
title_fullStr 5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
title_full_unstemmed 5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
title_short 5,5′-[(2,4-Dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
title_sort 5,5′-[(2,4-dichloro­phen­yl)methyl­ene]bis­(2,2-dimethyl-1,3-dioxane-4,6-dione)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3212288/
https://www.ncbi.nlm.nih.gov/pubmed/22090945
http://dx.doi.org/10.1107/S1600536811025384
work_keys_str_mv AT zengwulan 5524dichlorophenylmethylenebis22dimethyl13dioxane46dione

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