3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea

The thiono and carbonyl groups in the title compound, C(21)H(18)N(2)O(2)S, adopt an anti disposition with respect to the central C—N bond. The diphenyl­amine rings are twisted relative to each other by a dihedral angle of 82.55 (10)°. The 3-meth­oxy­benzoyl fragment is twisted relative to one of the...

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Detalles Bibliográficos
Autores principales: Md Nasir, Mohd Faizal, Hassan, Ibrahim N., M. Yamin, Bohari, Daud, W. R. W, Kassim, Mohammad B.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3212333/
https://www.ncbi.nlm.nih.gov/pubmed/22090990
http://dx.doi.org/10.1107/S1600536811025785
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author Md Nasir, Mohd Faizal
Hassan, Ibrahim N.
M. Yamin, Bohari
Daud, W. R. W
Kassim, Mohammad B.
author_facet Md Nasir, Mohd Faizal
Hassan, Ibrahim N.
M. Yamin, Bohari
Daud, W. R. W
Kassim, Mohammad B.
author_sort Md Nasir, Mohd Faizal
collection PubMed
description The thiono and carbonyl groups in the title compound, C(21)H(18)N(2)O(2)S, adopt an anti disposition with respect to the central C—N bond. The diphenyl­amine rings are twisted relative to each other by a dihedral angle of 82.55 (10)°. The 3-meth­oxy­benzoyl fragment is twisted relative to one of the diphenyl­amine rings, forming a dihedral angle of 74.04 (9)°. In the crystal, pairs of inter­molecular N—H⋯S hydrogen bonds link the mol­ecules into centrosymmetric dimers, forming columns parallel to the a axis.
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spelling pubmed-32123332011-11-16 3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea Md Nasir, Mohd Faizal Hassan, Ibrahim N. M. Yamin, Bohari Daud, W. R. W Kassim, Mohammad B. Acta Crystallogr Sect E Struct Rep Online Organic Papers The thiono and carbonyl groups in the title compound, C(21)H(18)N(2)O(2)S, adopt an anti disposition with respect to the central C—N bond. The diphenyl­amine rings are twisted relative to each other by a dihedral angle of 82.55 (10)°. The 3-meth­oxy­benzoyl fragment is twisted relative to one of the diphenyl­amine rings, forming a dihedral angle of 74.04 (9)°. In the crystal, pairs of inter­molecular N—H⋯S hydrogen bonds link the mol­ecules into centrosymmetric dimers, forming columns parallel to the a axis. International Union of Crystallography 2011-07-09 /pmc/articles/PMC3212333/ /pubmed/22090990 http://dx.doi.org/10.1107/S1600536811025785 Text en © Md Nasir et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Md Nasir, Mohd Faizal
Hassan, Ibrahim N.
M. Yamin, Bohari
Daud, W. R. W
Kassim, Mohammad B.
3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
title 3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
title_full 3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
title_fullStr 3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
title_full_unstemmed 3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
title_short 3-(3-Meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
title_sort 3-(3-meth­oxy­benzo­yl)-1,1-diphenyl­thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3212333/
https://www.ncbi.nlm.nih.gov/pubmed/22090990
http://dx.doi.org/10.1107/S1600536811025785
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