exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione

In the title compound, C(16)H(15)N(3)O(3), the dihedral angle between the approximately planar benzimidazolyl group (r.m.s. deviation = 0.010 Å) and the pyrrolidine ring is 78.20 (6)°. The C—C—N bond angle of the bridging CH(2) group is 112.14 (16)°. In the crystal, mol­ecules are linked via N—H⋯N h...

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Detalles Bibliográficos
Autores principales: Li, Shi-Kun, Zhang, Fan, Lv, Tian-Xi, Lin, Qiu-Yue
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213433/
https://www.ncbi.nlm.nih.gov/pubmed/22091012
http://dx.doi.org/10.1107/S1600536811026602
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author Li, Shi-Kun
Zhang, Fan
Lv, Tian-Xi
Lin, Qiu-Yue
author_facet Li, Shi-Kun
Zhang, Fan
Lv, Tian-Xi
Lin, Qiu-Yue
author_sort Li, Shi-Kun
collection PubMed
description In the title compound, C(16)H(15)N(3)O(3), the dihedral angle between the approximately planar benzimidazolyl group (r.m.s. deviation = 0.010 Å) and the pyrrolidine ring is 78.20 (6)°. The C—C—N bond angle of the bridging CH(2) group is 112.14 (16)°. In the crystal, mol­ecules are linked via N—H⋯N hydrogen bonds, forming infinite chains parallel to [101] and [10[Image: see text]].
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spelling pubmed-32134332011-11-16 exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione Li, Shi-Kun Zhang, Fan Lv, Tian-Xi Lin, Qiu-Yue Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(15)N(3)O(3), the dihedral angle between the approximately planar benzimidazolyl group (r.m.s. deviation = 0.010 Å) and the pyrrolidine ring is 78.20 (6)°. The C—C—N bond angle of the bridging CH(2) group is 112.14 (16)°. In the crystal, mol­ecules are linked via N—H⋯N hydrogen bonds, forming infinite chains parallel to [101] and [10[Image: see text]]. International Union of Crystallography 2011-07-09 /pmc/articles/PMC3213433/ /pubmed/22091012 http://dx.doi.org/10.1107/S1600536811026602 Text en © Li et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Shi-Kun
Zhang, Fan
Lv, Tian-Xi
Lin, Qiu-Yue
exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
title exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
title_full exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
title_fullStr exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
title_full_unstemmed exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
title_short exo-4-[(1H-Benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
title_sort exo-4-[(1h-benzimidazol-2-yl)meth­yl]-10-oxa-4-aza­tricyclo­[5.2.1.0(2,6)]decane-3,5-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213433/
https://www.ncbi.nlm.nih.gov/pubmed/22091012
http://dx.doi.org/10.1107/S1600536811026602
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