2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate

The title compound, C(10)H(8)N(4)O(4)·H(2)O, was obtained by the reaction of 5-hy­droxy-2-nitro­benzaldehyde with cyano­acetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 Å. In the crystal, mol...

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Detalles Bibliográficos
Autores principales: Li, Hongbo, Ni, Xiaocheng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213457/
https://www.ncbi.nlm.nih.gov/pubmed/22091036
http://dx.doi.org/10.1107/S1600536811025463
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author Li, Hongbo
Ni, Xiaocheng
author_facet Li, Hongbo
Ni, Xiaocheng
author_sort Li, Hongbo
collection PubMed
description The title compound, C(10)H(8)N(4)O(4)·H(2)O, was obtained by the reaction of 5-hy­droxy-2-nitro­benzaldehyde with cyano­acetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 Å. In the crystal, mol­ecules are linked by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, generating a three-dimensional network.
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spelling pubmed-32134572011-11-16 2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate Li, Hongbo Ni, Xiaocheng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(8)N(4)O(4)·H(2)O, was obtained by the reaction of 5-hy­droxy-2-nitro­benzaldehyde with cyano­acetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 Å. In the crystal, mol­ecules are linked by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, generating a three-dimensional network. International Union of Crystallography 2011-07-09 /pmc/articles/PMC3213457/ /pubmed/22091036 http://dx.doi.org/10.1107/S1600536811025463 Text en © Li and Ni 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Hongbo
Ni, Xiaocheng
2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
title 2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
title_full 2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
title_fullStr 2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
title_full_unstemmed 2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
title_short 2-Cyano-N′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
title_sort 2-cyano-n′-(5-hy­droxy-2-nitro­benzyl­idene)acetohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213457/
https://www.ncbi.nlm.nih.gov/pubmed/22091036
http://dx.doi.org/10.1107/S1600536811025463
work_keys_str_mv AT lihongbo 2cyanon5hydroxy2nitrobenzylideneacetohydrazidemonohydrate
AT nixiaocheng 2cyanon5hydroxy2nitrobenzylideneacetohydrazidemonohydrate

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