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N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide
The asymmetric unit of the title compound, C(17)H(17)ClN(2)O(2), contains one half-molecule with a center of inversion at the mid-point of the central C—C bond. The amide N—H group is anti to the meta-chloro/methyl groups in the adjacent benzene rings. The dihedral angle between the benzene ring an...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213520/ https://www.ncbi.nlm.nih.gov/pubmed/22091099 http://dx.doi.org/10.1107/S1600536811028121 |
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author | Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme |
author_facet | Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme |
author_sort | Saraswathi, B. S. |
collection | PubMed |
description | The asymmetric unit of the title compound, C(17)H(17)ClN(2)O(2), contains one half-molecule with a center of inversion at the mid-point of the central C—C bond. The amide N—H group is anti to the meta-chloro/methyl groups in the adjacent benzene rings. The dihedral angle between the benzene ring and the NH—C(O)—CH(2) segment is 43.5 (1)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains along the a axis. The methyl group and the Cl atom occupy the same position and were treated in a disorder model with site-occupation factors of 0.5 each. |
format | Online Article Text |
id | pubmed-3213520 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-32135202011-11-16 N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(17)H(17)ClN(2)O(2), contains one half-molecule with a center of inversion at the mid-point of the central C—C bond. The amide N—H group is anti to the meta-chloro/methyl groups in the adjacent benzene rings. The dihedral angle between the benzene ring and the NH—C(O)—CH(2) segment is 43.5 (1)°. In the crystal, intermolecular N—H⋯O hydrogen bonds link the molecules into chains along the a axis. The methyl group and the Cl atom occupy the same position and were treated in a disorder model with site-occupation factors of 0.5 each. International Union of Crystallography 2011-07-23 /pmc/articles/PMC3213520/ /pubmed/22091099 http://dx.doi.org/10.1107/S1600536811028121 Text en © Saraswathi et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide |
title |
N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide |
title_full |
N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide |
title_fullStr |
N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide |
title_full_unstemmed |
N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide |
title_short |
N-(3-Chlorophenyl)-N′-(3-methylphenyl)succinamide |
title_sort | n-(3-chlorophenyl)-n′-(3-methylphenyl)succinamide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213520/ https://www.ncbi.nlm.nih.gov/pubmed/22091099 http://dx.doi.org/10.1107/S1600536811028121 |
work_keys_str_mv | AT saraswathibs n3chlorophenyln3methylphenylsuccinamide AT forosabine n3chlorophenyln3methylphenylsuccinamide AT gowdabthimme n3chlorophenyln3methylphenylsuccinamide |