N-(2,5-Dichloro­phen­yl)succinamic acid

In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, inter­molecular O—H⋯O and N—H⋯O hydrogen bonds pack the mol­ecules into two types of chains alo...

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Detalles Bibliográficos
Autores principales: Saraswathi, B. S., Foro, Sabine, Gowda, B. Thimme
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213535/
https://www.ncbi.nlm.nih.gov/pubmed/22091112
http://dx.doi.org/10.1107/S1600536811028297
Descripción
Sumario:In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, inter­molecular O—H⋯O and N—H⋯O hydrogen bonds pack the mol­ecules into two types of chains along the a and b axes, respectively, leading to an overall sheet structure. The acid group in the side chain is disordered and was refined using a split model with site-occupation factors of 0.60:0.40.

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