N-(2,5-Dichloro­phen­yl)succinamic acid

In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, inter­molecular O—H⋯O and N—H⋯O hydrogen bonds pack the mol­ecules into two types of chains alo...

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Detalles Bibliográficos
Autores principales: Saraswathi, B. S., Foro, Sabine, Gowda, B. Thimme
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213535/
https://www.ncbi.nlm.nih.gov/pubmed/22091112
http://dx.doi.org/10.1107/S1600536811028297
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author Saraswathi, B. S.
Foro, Sabine
Gowda, B. Thimme
author_facet Saraswathi, B. S.
Foro, Sabine
Gowda, B. Thimme
author_sort Saraswathi, B. S.
collection PubMed
description In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, inter­molecular O—H⋯O and N—H⋯O hydrogen bonds pack the mol­ecules into two types of chains along the a and b axes, respectively, leading to an overall sheet structure. The acid group in the side chain is disordered and was refined using a split model with site-occupation factors of 0.60:0.40.
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spelling pubmed-32135352011-11-16 N-(2,5-Dichloro­phen­yl)succinamic acid Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, inter­molecular O—H⋯O and N—H⋯O hydrogen bonds pack the mol­ecules into two types of chains along the a and b axes, respectively, leading to an overall sheet structure. The acid group in the side chain is disordered and was refined using a split model with site-occupation factors of 0.60:0.40. International Union of Crystallography 2011-07-23 /pmc/articles/PMC3213535/ /pubmed/22091112 http://dx.doi.org/10.1107/S1600536811028297 Text en © Saraswathi et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saraswathi, B. S.
Foro, Sabine
Gowda, B. Thimme
N-(2,5-Dichloro­phen­yl)succinamic acid
title N-(2,5-Dichloro­phen­yl)succinamic acid
title_full N-(2,5-Dichloro­phen­yl)succinamic acid
title_fullStr N-(2,5-Dichloro­phen­yl)succinamic acid
title_full_unstemmed N-(2,5-Dichloro­phen­yl)succinamic acid
title_short N-(2,5-Dichloro­phen­yl)succinamic acid
title_sort n-(2,5-dichloro­phen­yl)succinamic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213535/
https://www.ncbi.nlm.nih.gov/pubmed/22091112
http://dx.doi.org/10.1107/S1600536811028297
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