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N-(2,5-Dichlorophenyl)succinamic acid
In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, intermolecular O—H⋯O and N—H⋯O hydrogen bonds pack the molecules into two types of chains alo...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213535/ https://www.ncbi.nlm.nih.gov/pubmed/22091112 http://dx.doi.org/10.1107/S1600536811028297 |
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author | Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme |
author_facet | Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme |
author_sort | Saraswathi, B. S. |
collection | PubMed |
description | In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, intermolecular O—H⋯O and N—H⋯O hydrogen bonds pack the molecules into two types of chains along the a and b axes, respectively, leading to an overall sheet structure. The acid group in the side chain is disordered and was refined using a split model with site-occupation factors of 0.60:0.40. |
format | Online Article Text |
id | pubmed-3213535 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-32135352011-11-16 N-(2,5-Dichlorophenyl)succinamic acid Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(9)Cl(2)NO(3), the conformation of the N—H bond in the amide segment is syn with respect to the ortho-Cl atom and anti to the meta-Cl atom of the benzene ring. In the crystal, intermolecular O—H⋯O and N—H⋯O hydrogen bonds pack the molecules into two types of chains along the a and b axes, respectively, leading to an overall sheet structure. The acid group in the side chain is disordered and was refined using a split model with site-occupation factors of 0.60:0.40. International Union of Crystallography 2011-07-23 /pmc/articles/PMC3213535/ /pubmed/22091112 http://dx.doi.org/10.1107/S1600536811028297 Text en © Saraswathi et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Saraswathi, B. S. Foro, Sabine Gowda, B. Thimme N-(2,5-Dichlorophenyl)succinamic acid |
title |
N-(2,5-Dichlorophenyl)succinamic acid |
title_full |
N-(2,5-Dichlorophenyl)succinamic acid |
title_fullStr |
N-(2,5-Dichlorophenyl)succinamic acid |
title_full_unstemmed |
N-(2,5-Dichlorophenyl)succinamic acid |
title_short |
N-(2,5-Dichlorophenyl)succinamic acid |
title_sort | n-(2,5-dichlorophenyl)succinamic acid |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213535/ https://www.ncbi.nlm.nih.gov/pubmed/22091112 http://dx.doi.org/10.1107/S1600536811028297 |
work_keys_str_mv | AT saraswathibs n25dichlorophenylsuccinamicacid AT forosabine n25dichlorophenylsuccinamicacid AT gowdabthimme n25dichlorophenylsuccinamicacid |