1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate

In the title compound, C(17)H(18)N(4)O(2)S·CH(3)OH, the two benzene rings in the thio­carbonohydrazide mol­ecule form a dihedral angle of 22.42 (18)°. Pairs of N—H⋯S hydrogen bonds link thio­carbonohydrazide mol­ecules into centrosymmetric dimers. Methanol solvent mol­ecules serve as donors (O—H⋯S a...

Descripción completa

Detalles Bibliográficos
Autor principal: Zhao, Xinyu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213573/
https://www.ncbi.nlm.nih.gov/pubmed/22091150
http://dx.doi.org/10.1107/S1600536811029035
_version_ 1782216154040762368
author Zhao, Xinyu
author_facet Zhao, Xinyu
author_sort Zhao, Xinyu
collection PubMed
description In the title compound, C(17)H(18)N(4)O(2)S·CH(3)OH, the two benzene rings in the thio­carbonohydrazide mol­ecule form a dihedral angle of 22.42 (18)°. Pairs of N—H⋯S hydrogen bonds link thio­carbonohydrazide mol­ecules into centrosymmetric dimers. Methanol solvent mol­ecules serve as donors (O—H⋯S and O—H⋯N) and acceptors (N—H⋯O and C—H⋯O) of weak inter­molecular hydrogen bonds, which link further these dimers into double ribbons along the b axis.
format Online
Article
Text
id pubmed-3213573
institution National Center for Biotechnology Information
language English
publishDate 2011
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32135732011-11-16 1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate Zhao, Xinyu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(17)H(18)N(4)O(2)S·CH(3)OH, the two benzene rings in the thio­carbonohydrazide mol­ecule form a dihedral angle of 22.42 (18)°. Pairs of N—H⋯S hydrogen bonds link thio­carbonohydrazide mol­ecules into centrosymmetric dimers. Methanol solvent mol­ecules serve as donors (O—H⋯S and O—H⋯N) and acceptors (N—H⋯O and C—H⋯O) of weak inter­molecular hydrogen bonds, which link further these dimers into double ribbons along the b axis. International Union of Crystallography 2011-07-23 /pmc/articles/PMC3213573/ /pubmed/22091150 http://dx.doi.org/10.1107/S1600536811029035 Text en © Xinyu Zhao 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Xinyu
1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title 1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_full 1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_fullStr 1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_full_unstemmed 1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_short 1,5-Bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
title_sort 1,5-bis(4-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213573/
https://www.ncbi.nlm.nih.gov/pubmed/22091150
http://dx.doi.org/10.1107/S1600536811029035
work_keys_str_mv AT zhaoxinyu 15bis4methoxybenzylidenethiocarbonohydrazidemethanolmonosolvate

Ejemplares similares