2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile

The title compound, C(17)H(14)N(2)O(2)S, crystallizes with two roughly planar mol­ecules in the asymmetric unit, in which the dihedral angles between the 1,3-benzodioxole-5-carbaldehyde moiety and the heterocyclic five-membered ring are 3.76 (5) and 5.33 (12)°. In each mol­ecule, a short C—H⋯S conta...

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Detalles Bibliográficos
Autores principales: Asiri, Abdullah M., Khan, Salman A., Tahir, M. Nawaz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213598/
https://www.ncbi.nlm.nih.gov/pubmed/22091175
http://dx.doi.org/10.1107/S1600536811029564
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author Asiri, Abdullah M.
Khan, Salman A.
Tahir, M. Nawaz
author_facet Asiri, Abdullah M.
Khan, Salman A.
Tahir, M. Nawaz
author_sort Asiri, Abdullah M.
collection PubMed
description The title compound, C(17)H(14)N(2)O(2)S, crystallizes with two roughly planar mol­ecules in the asymmetric unit, in which the dihedral angles between the 1,3-benzodioxole-5-carbaldehyde moiety and the heterocyclic five-membered ring are 3.76 (5) and 5.33 (12)°. In each mol­ecule, a short C—H⋯S contact generates an S(5) ring. In the crystal, pairs of mol­ecules are linked by a weak C—H⋯N inter­action, forming dimers.
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spelling pubmed-32135982011-11-16 2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile Asiri, Abdullah M. Khan, Salman A. Tahir, M. Nawaz Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(14)N(2)O(2)S, crystallizes with two roughly planar mol­ecules in the asymmetric unit, in which the dihedral angles between the 1,3-benzodioxole-5-carbaldehyde moiety and the heterocyclic five-membered ring are 3.76 (5) and 5.33 (12)°. In each mol­ecule, a short C—H⋯S contact generates an S(5) ring. In the crystal, pairs of mol­ecules are linked by a weak C—H⋯N inter­action, forming dimers. International Union of Crystallography 2011-07-30 /pmc/articles/PMC3213598/ /pubmed/22091175 http://dx.doi.org/10.1107/S1600536811029564 Text en © Asiri et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Asiri, Abdullah M.
Khan, Salman A.
Tahir, M. Nawaz
2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
title 2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
title_full 2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
title_fullStr 2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
title_full_unstemmed 2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
title_short 2-[(1,3-Benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
title_sort 2-[(1,3-benzodioxol-5-yl­methyl­idene)amino]-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carbonitrile
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213598/
https://www.ncbi.nlm.nih.gov/pubmed/22091175
http://dx.doi.org/10.1107/S1600536811029564
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AT khansalmana 213benzodioxol5ylmethylideneamino4567tetrahydro1benzothiophene3carbonitrile
AT tahirmnawaz 213benzodioxol5ylmethylideneamino4567tetrahydro1benzothiophene3carbonitrile

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