N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide

In the title compound, C(18)H(18)Cl(2)N(2)O(6)S(2), the asymmetric unit contains half a mol­ecule with a center of symmetry at the mid-point of the central C—C bond. The dihedral angle between the benzene ring and the SO(2)—NH—C(O) segment in the two halves of the mol­ecule is 83.5 (2)°. In the crys...

Descripción completa

Detalles Bibliográficos
Autores principales: Rodrigues, Vinola Z., Foro, Sabine, Gowda, B. Thimme
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213613/
https://www.ncbi.nlm.nih.gov/pubmed/22091190
http://dx.doi.org/10.1107/S1600536811030029
_version_ 1782216163075293184
author Rodrigues, Vinola Z.
Foro, Sabine
Gowda, B. Thimme
author_facet Rodrigues, Vinola Z.
Foro, Sabine
Gowda, B. Thimme
author_sort Rodrigues, Vinola Z.
collection PubMed
description In the title compound, C(18)H(18)Cl(2)N(2)O(6)S(2), the asymmetric unit contains half a mol­ecule with a center of symmetry at the mid-point of the central C—C bond. The dihedral angle between the benzene ring and the SO(2)—NH—C(O) segment in the two halves of the mol­ecule is 83.5 (2)°. In the crystal, N—H⋯O(S) inter­molecular hydrogen bonds link the mol­ecules into infinite chains running along the c axis. The O atom involved in the hydrogen bond has a longer S—O bond than the other O atom bonded to S [1.403 (4) versus 1.361 (4) Å].
format Online
Article
Text
id pubmed-3213613
institution National Center for Biotechnology Information
language English
publishDate 2011
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32136132011-11-16 N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide Rodrigues, Vinola Z. Foro, Sabine Gowda, B. Thimme Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(18)H(18)Cl(2)N(2)O(6)S(2), the asymmetric unit contains half a mol­ecule with a center of symmetry at the mid-point of the central C—C bond. The dihedral angle between the benzene ring and the SO(2)—NH—C(O) segment in the two halves of the mol­ecule is 83.5 (2)°. In the crystal, N—H⋯O(S) inter­molecular hydrogen bonds link the mol­ecules into infinite chains running along the c axis. The O atom involved in the hydrogen bond has a longer S—O bond than the other O atom bonded to S [1.403 (4) versus 1.361 (4) Å]. International Union of Crystallography 2011-07-30 /pmc/articles/PMC3213613/ /pubmed/22091190 http://dx.doi.org/10.1107/S1600536811030029 Text en © Rodrigues et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rodrigues, Vinola Z.
Foro, Sabine
Gowda, B. Thimme
N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide
title N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide
title_full N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide
title_fullStr N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide
title_full_unstemmed N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide
title_short N,N′-Bis(4-chloro­phenyl­sulfon­yl)­adipamide
title_sort n,n′-bis(4-chloro­phenyl­sulfon­yl)­adipamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3213613/
https://www.ncbi.nlm.nih.gov/pubmed/22091190
http://dx.doi.org/10.1107/S1600536811030029
work_keys_str_mv AT rodriguesvinolaz nnbis4chlorophenylsulfonyladipamide
AT forosabine nnbis4chlorophenylsulfonyladipamide
AT gowdabthimme nnbis4chlorophenylsulfonyladipamide

Ejemplares similares