Morpholinium hydrogen chloranilate methanol monosolvate

In the crystal structure of the title compound, C(4)H(10)NO(+)·C(6)HCl(2)O(4) (−)·CH(4)O, the components are held together by bifurcated O—H⋯(O,O), O—H⋯(O,Cl) and N—H⋯(O,O) hydrogen bonds into a centrosymmetric 2+2+2 aggregate. The aggregates are further connected by another bifurcated N—H⋯(O, O) hy...

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Detalles Bibliográficos
Autores principales: Gotoh, Kazuma, Tahara, Yuki, Ishida, Hiroyuki
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3238982/
https://www.ncbi.nlm.nih.gov/pubmed/22199831
http://dx.doi.org/10.1107/S1600536811047891
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author Gotoh, Kazuma
Tahara, Yuki
Ishida, Hiroyuki
author_facet Gotoh, Kazuma
Tahara, Yuki
Ishida, Hiroyuki
author_sort Gotoh, Kazuma
collection PubMed
description In the crystal structure of the title compound, C(4)H(10)NO(+)·C(6)HCl(2)O(4) (−)·CH(4)O, the components are held together by bifurcated O—H⋯(O,O), O—H⋯(O,Cl) and N—H⋯(O,O) hydrogen bonds into a centrosymmetric 2+2+2 aggregate. The aggregates are further connected by another bifurcated N—H⋯(O, O) hydrogen bond, forming a double-tape structure along the b axis. A weak C—H⋯O inter­action is observed between the tapes.
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spelling pubmed-32389822011-12-23 Morpholinium hydrogen chloranilate methanol monosolvate Gotoh, Kazuma Tahara, Yuki Ishida, Hiroyuki Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(4)H(10)NO(+)·C(6)HCl(2)O(4) (−)·CH(4)O, the components are held together by bifurcated O—H⋯(O,O), O—H⋯(O,Cl) and N—H⋯(O,O) hydrogen bonds into a centrosymmetric 2+2+2 aggregate. The aggregates are further connected by another bifurcated N—H⋯(O, O) hydrogen bond, forming a double-tape structure along the b axis. A weak C—H⋯O inter­action is observed between the tapes. International Union of Crystallography 2011-11-16 /pmc/articles/PMC3238982/ /pubmed/22199831 http://dx.doi.org/10.1107/S1600536811047891 Text en © Gotoh et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gotoh, Kazuma
Tahara, Yuki
Ishida, Hiroyuki
Morpholinium hydrogen chloranilate methanol monosolvate
title Morpholinium hydrogen chloranilate methanol monosolvate
title_full Morpholinium hydrogen chloranilate methanol monosolvate
title_fullStr Morpholinium hydrogen chloranilate methanol monosolvate
title_full_unstemmed Morpholinium hydrogen chloranilate methanol monosolvate
title_short Morpholinium hydrogen chloranilate methanol monosolvate
title_sort morpholinium hydrogen chloranilate methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3238982/
https://www.ncbi.nlm.nih.gov/pubmed/22199831
http://dx.doi.org/10.1107/S1600536811047891
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AT taharayuki morpholiniumhydrogenchloranilatemethanolmonosolvate
AT ishidahiroyuki morpholiniumhydrogenchloranilatemethanolmonosolvate

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