1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea

In the title compound, C(13)H(18)N(2)O(2)S, the 4-meth­oxy­benzoyl fragment is approximately planar [maximum deviation = 0.057 (2) Å] and twisted relative to the thio­amide fragment, forming a dihedral angle of 86.62 (6)°. The two Csp (2)—Nsp (2) bonds in the thio­urea unit differ significantly in l...

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Autores principales: Al-abbasi, Aisha A., Mohamed Tahir, Mohamed Ibrahim, Kassim, Mohammad B.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239051/
https://www.ncbi.nlm.nih.gov/pubmed/22199899
http://dx.doi.org/10.1107/S1600536811049208
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author Al-abbasi, Aisha A.
Mohamed Tahir, Mohamed Ibrahim
Kassim, Mohammad B.
author_facet Al-abbasi, Aisha A.
Mohamed Tahir, Mohamed Ibrahim
Kassim, Mohammad B.
author_sort Al-abbasi, Aisha A.
collection PubMed
description In the title compound, C(13)H(18)N(2)O(2)S, the 4-meth­oxy­benzoyl fragment is approximately planar [maximum deviation = 0.057 (2) Å] and twisted relative to the thio­amide fragment, forming a dihedral angle of 86.62 (6)°. The two Csp (2)—Nsp (2) bonds in the thio­urea unit differ significantly in length [1.327 (2) and 1.431 (2) Å]. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into chains parallel to [010].
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spelling pubmed-32390512011-12-23 1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea Al-abbasi, Aisha A. Mohamed Tahir, Mohamed Ibrahim Kassim, Mohammad B. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(18)N(2)O(2)S, the 4-meth­oxy­benzoyl fragment is approximately planar [maximum deviation = 0.057 (2) Å] and twisted relative to the thio­amide fragment, forming a dihedral angle of 86.62 (6)°. The two Csp (2)—Nsp (2) bonds in the thio­urea unit differ significantly in length [1.327 (2) and 1.431 (2) Å]. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into chains parallel to [010]. International Union of Crystallography 2011-11-25 /pmc/articles/PMC3239051/ /pubmed/22199899 http://dx.doi.org/10.1107/S1600536811049208 Text en © Al-abbasi et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Al-abbasi, Aisha A.
Mohamed Tahir, Mohamed Ibrahim
Kassim, Mohammad B.
1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
title 1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
title_full 1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
title_fullStr 1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
title_full_unstemmed 1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
title_short 1,1-Diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
title_sort 1,1-diethyl-3-(4-meth­oxy­benzo­yl)thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239051/
https://www.ncbi.nlm.nih.gov/pubmed/22199899
http://dx.doi.org/10.1107/S1600536811049208
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AT mohamedtahirmohamedibrahim 11diethyl34methoxybenzoylthiourea
AT kassimmohammadb 11diethyl34methoxybenzoylthiourea

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