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Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate

In the title hydrate, C(16)H(19)N(3)O(3)·1.5H(2)O, both water mol­ecules are disordered: one over two adjacent sites in a 0.498 (5):0.502 (5) ratio and one lying near a crystallographic twofold axis. The dihedral angle between the pyridine rings of the organic moleucle is 1.47 (6)°. In the crystal,...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Hemamalini, Madhukar, Hazra, Anita, Goswami, Shyamaprosad
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239052/
https://www.ncbi.nlm.nih.gov/pubmed/22199900
http://dx.doi.org/10.1107/S160053681104921X
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author Fun, Hoong-Kun
Hemamalini, Madhukar
Hazra, Anita
Goswami, Shyamaprosad
author_facet Fun, Hoong-Kun
Hemamalini, Madhukar
Hazra, Anita
Goswami, Shyamaprosad
author_sort Fun, Hoong-Kun
collection PubMed
description In the title hydrate, C(16)H(19)N(3)O(3)·1.5H(2)O, both water mol­ecules are disordered: one over two adjacent sites in a 0.498 (5):0.502 (5) ratio and one lying near a crystallographic twofold axis. The dihedral angle between the pyridine rings of the organic moleucle is 1.47 (6)°. In the crystal, the components are linked by N—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds, forming sheets lying parallel to the ac plane.
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spelling pubmed-32390522011-12-23 Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate Fun, Hoong-Kun Hemamalini, Madhukar Hazra, Anita Goswami, Shyamaprosad Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title hydrate, C(16)H(19)N(3)O(3)·1.5H(2)O, both water mol­ecules are disordered: one over two adjacent sites in a 0.498 (5):0.502 (5) ratio and one lying near a crystallographic twofold axis. The dihedral angle between the pyridine rings of the organic moleucle is 1.47 (6)°. In the crystal, the components are linked by N—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds, forming sheets lying parallel to the ac plane. International Union of Crystallography 2011-11-25 /pmc/articles/PMC3239052/ /pubmed/22199900 http://dx.doi.org/10.1107/S160053681104921X Text en © Fun et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Hemamalini, Madhukar
Hazra, Anita
Goswami, Shyamaprosad
Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
title Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
title_full Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
title_fullStr Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
title_full_unstemmed Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
title_short Ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
title_sort ethyl 7-pivaloyl­amino-1,8-naphthyridine-2-carboxyl­ate sesquihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239052/
https://www.ncbi.nlm.nih.gov/pubmed/22199900
http://dx.doi.org/10.1107/S160053681104921X
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