2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)

The asymmetric unit of the title compound, C(5)H(8)N(3) (+)·C(7)H(4)ClO(2) (−)·C(7)H(5)ClO(2), contains an ion pair and a 3-chloro­benzoic acid mol­ecule. In the cation, the pyridine N atom is protonated. In the crystal, the components are connected via N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds, thereby...

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Detalles Bibliográficos
Autores principales: Hemamalini, Madhukar, Goh, Jia Hao, Fun, Hoong-Kun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239122/
https://www.ncbi.nlm.nih.gov/pubmed/22199970
http://dx.doi.org/10.1107/S1600536811050422
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author Hemamalini, Madhukar
Goh, Jia Hao
Fun, Hoong-Kun
author_facet Hemamalini, Madhukar
Goh, Jia Hao
Fun, Hoong-Kun
author_sort Hemamalini, Madhukar
collection PubMed
description The asymmetric unit of the title compound, C(5)H(8)N(3) (+)·C(7)H(4)ClO(2) (−)·C(7)H(5)ClO(2), contains an ion pair and a 3-chloro­benzoic acid mol­ecule. In the cation, the pyridine N atom is protonated. In the crystal, the components are connected via N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds, thereby forming sheets lying parallel to (100).
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spelling pubmed-32391222011-12-23 2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1) Hemamalini, Madhukar Goh, Jia Hao Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(5)H(8)N(3) (+)·C(7)H(4)ClO(2) (−)·C(7)H(5)ClO(2), contains an ion pair and a 3-chloro­benzoic acid mol­ecule. In the cation, the pyridine N atom is protonated. In the crystal, the components are connected via N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds, thereby forming sheets lying parallel to (100). International Union of Crystallography 2011-11-30 /pmc/articles/PMC3239122/ /pubmed/22199970 http://dx.doi.org/10.1107/S1600536811050422 Text en © Hemamalini et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hemamalini, Madhukar
Goh, Jia Hao
Fun, Hoong-Kun
2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
title 2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
title_full 2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
title_fullStr 2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
title_full_unstemmed 2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
title_short 2,3-Diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
title_sort 2,3-diamino­pyridinium 3-chloro­benzo­ate–3-chloro­benzoic acid (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239122/
https://www.ncbi.nlm.nih.gov/pubmed/22199970
http://dx.doi.org/10.1107/S1600536811050422
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