5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide

In the title compound, C(16)H(16)N(4)OS, the dihedral angle between the pyridine and benzene rings is 81.08 (6)°. The pyrazole ring makes dihedral angles of 12.36 (7) and 87.96 (6)°, respectively, with the pyridine and benzene rings. In the crystal, mol­ecules are linked by N—H⋯O and N—H⋯S hydrogen...

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Autores principales: Nonthason, Phonpawee, Suwunwong, Thitipone, Chantrapromma, Suchada, Fun, Hoong-Kun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239124/
https://www.ncbi.nlm.nih.gov/pubmed/22199972
http://dx.doi.org/10.1107/S1600536811050033
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author Nonthason, Phonpawee
Suwunwong, Thitipone
Chantrapromma, Suchada
Fun, Hoong-Kun
author_facet Nonthason, Phonpawee
Suwunwong, Thitipone
Chantrapromma, Suchada
Fun, Hoong-Kun
author_sort Nonthason, Phonpawee
collection PubMed
description In the title compound, C(16)H(16)N(4)OS, the dihedral angle between the pyridine and benzene rings is 81.08 (6)°. The pyrazole ring makes dihedral angles of 12.36 (7) and 87.96 (6)°, respectively, with the pyridine and benzene rings. In the crystal, mol­ecules are linked by N—H⋯O and N—H⋯S hydrogen bonds and a weak C—H⋯S inter­action into a layer parallel to the ab plane. Weak C—H⋯π and π–π inter­actions [centroid–centroid distances = 3.7043 (9) and 3.8120 (7) Å] are also observed.
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spelling pubmed-32391242011-12-23 5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide Nonthason, Phonpawee Suwunwong, Thitipone Chantrapromma, Suchada Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(16)N(4)OS, the dihedral angle between the pyridine and benzene rings is 81.08 (6)°. The pyrazole ring makes dihedral angles of 12.36 (7) and 87.96 (6)°, respectively, with the pyridine and benzene rings. In the crystal, mol­ecules are linked by N—H⋯O and N—H⋯S hydrogen bonds and a weak C—H⋯S inter­action into a layer parallel to the ab plane. Weak C—H⋯π and π–π inter­actions [centroid–centroid distances = 3.7043 (9) and 3.8120 (7) Å] are also observed. International Union of Crystallography 2011-11-30 /pmc/articles/PMC3239124/ /pubmed/22199972 http://dx.doi.org/10.1107/S1600536811050033 Text en © Nonthason et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Nonthason, Phonpawee
Suwunwong, Thitipone
Chantrapromma, Suchada
Fun, Hoong-Kun
5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title 5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_full 5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_fullStr 5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_full_unstemmed 5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_short 5-(4-Meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1H-pyrazole-1-carbothio­amide
title_sort 5-(4-meth­oxy­phen­yl)-3-(pyridin-2-yl)-4,5-dihydro-1h-pyrazole-1-carbothio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239124/
https://www.ncbi.nlm.nih.gov/pubmed/22199972
http://dx.doi.org/10.1107/S1600536811050033
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AT chantraprommasuchada 54methoxyphenyl3pyridin2yl45dihydro1hpyrazole1carbothioamide
AT funhoongkun 54methoxyphenyl3pyridin2yl45dihydro1hpyrazole1carbothioamide

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