(E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione

In the title compound, C(10)H(9)N(3)O(2)S(2), the dihedral angle between the benzene ring and the five-membered ring is 1.54 (13)°. An intra­molecular O—H⋯N hydrogen bond makes an S(6) ring. In the crystal, mol­ecules are linked together through bifurcated N—H⋯(O,O) hydrogen bonds having R (1) (2)(5...

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Detalles Bibliográficos
Autores principales: Kargar, Hadi, Kia, Reza
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239138/
https://www.ncbi.nlm.nih.gov/pubmed/22199986
http://dx.doi.org/10.1107/S1600536811050902
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author Kargar, Hadi
Kia, Reza
author_facet Kargar, Hadi
Kia, Reza
author_sort Kargar, Hadi
collection PubMed
description In the title compound, C(10)H(9)N(3)O(2)S(2), the dihedral angle between the benzene ring and the five-membered ring is 1.54 (13)°. An intra­molecular O—H⋯N hydrogen bond makes an S(6) ring. In the crystal, mol­ecules are linked together through bifurcated N—H⋯(O,O) hydrogen bonds having R (1) (2)(5) ring motifs, forming chains along the b axis. The crystal structure also features π–π inter­actions, with centroid–centroid distances of 3.699 (3)–3.767 (3) Å.
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spelling pubmed-32391382011-12-23 (E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione Kargar, Hadi Kia, Reza Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(9)N(3)O(2)S(2), the dihedral angle between the benzene ring and the five-membered ring is 1.54 (13)°. An intra­molecular O—H⋯N hydrogen bond makes an S(6) ring. In the crystal, mol­ecules are linked together through bifurcated N—H⋯(O,O) hydrogen bonds having R (1) (2)(5) ring motifs, forming chains along the b axis. The crystal structure also features π–π inter­actions, with centroid–centroid distances of 3.699 (3)–3.767 (3) Å. International Union of Crystallography 2011-11-30 /pmc/articles/PMC3239138/ /pubmed/22199986 http://dx.doi.org/10.1107/S1600536811050902 Text en © Kargar and Kia 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Kargar, Hadi
Kia, Reza
(E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione
title (E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione
title_full (E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione
title_fullStr (E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione
title_full_unstemmed (E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione
title_short (E)-5-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3H)-thione
title_sort (e)-5-[(2-hy­droxy-3-meth­oxy­benzyl­idene)amino]-1,3,4-thia­diazole-2(3h)-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3239138/
https://www.ncbi.nlm.nih.gov/pubmed/22199986
http://dx.doi.org/10.1107/S1600536811050902
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