Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template

Superfine powders of poly (methyl methacrylate) (PMMA) have been prepared by means of an emulsion polymerization method. These have been used as templates in the synthesis of tetragonal phase mesoporous zirconia by the sol–gel method, using zirconium oxychloride and oxalic acid as raw materials. The...

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Detalles Bibliográficos
Autores principales: Duan, Guorong, Zhang, Chunxiang, Li, Aimei, Yang, Xujie, Lu, Lude, Wang, Xin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer 2008
Materias:
Nano Express
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3244794/
https://www.ncbi.nlm.nih.gov/pubmed/21787437
http://dx.doi.org/10.1007/s11671-008-9123-7
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author Duan, Guorong
Zhang, Chunxiang
Li, Aimei
Yang, Xujie
Lu, Lude
Wang, Xin
author_facet Duan, Guorong
Zhang, Chunxiang
Li, Aimei
Yang, Xujie
Lu, Lude
Wang, Xin
author_sort Duan, Guorong
collection PubMed
description Superfine powders of poly (methyl methacrylate) (PMMA) have been prepared by means of an emulsion polymerization method. These have been used as templates in the synthesis of tetragonal phase mesoporous zirconia by the sol–gel method, using zirconium oxychloride and oxalic acid as raw materials. The products have been characterized by infrared spectroscopy, X-ray diffraction analysis, transmission electron microscopy, N(2)adsorption-desorption isotherms, and pore size distribution. The results indicate that the average pore size was found to be 3.7 nm.
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spelling pubmed-32447942011-12-29 Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template Duan, Guorong Zhang, Chunxiang Li, Aimei Yang, Xujie Lu, Lude Wang, Xin Nanoscale Res Lett Nano Express Superfine powders of poly (methyl methacrylate) (PMMA) have been prepared by means of an emulsion polymerization method. These have been used as templates in the synthesis of tetragonal phase mesoporous zirconia by the sol–gel method, using zirconium oxychloride and oxalic acid as raw materials. The products have been characterized by infrared spectroscopy, X-ray diffraction analysis, transmission electron microscopy, N(2)adsorption-desorption isotherms, and pore size distribution. The results indicate that the average pore size was found to be 3.7 nm. Springer 2008-02-28 /pmc/articles/PMC3244794/ /pubmed/21787437 http://dx.doi.org/10.1007/s11671-008-9123-7 Text en Copyright ©2008 to the authors
spellingShingle Nano Express
Duan, Guorong
Zhang, Chunxiang
Li, Aimei
Yang, Xujie
Lu, Lude
Wang, Xin
Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template
title Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template
title_full Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template
title_fullStr Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template
title_full_unstemmed Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template
title_short Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template
title_sort preparation and characterization of mesoporous zirconia made by using a poly (methyl methacrylate) template
topic Nano Express
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3244794/
https://www.ncbi.nlm.nih.gov/pubmed/21787437
http://dx.doi.org/10.1007/s11671-008-9123-7
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