Cargando…

Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]

The title compound, [Li(4)O(4)(C(12)H(8)BO)(4)(C(4)H(10)O)(4)], features a Li(4)O(4) cube. Each Li atom in the cube is additionally coordinated by a diethyl ether mol­ecule and each O atom in the cube carries a 9-oxa-10-boraanthracene residue. The crystal studied was a non-merohedral twin [twin law...

Descripción completa

Detalles Bibliográficos
Autores principales: Franz, Daniel, Lerner, Hans-Wolfram, Büttner, Dominik, Bolte, Michael
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3246952/
https://www.ncbi.nlm.nih.gov/pubmed/22219772
http://dx.doi.org/10.1107/S1600536811041201
_version_ 1782220011674271744
author Franz, Daniel
Lerner, Hans-Wolfram
Büttner, Dominik
Bolte, Michael
author_facet Franz, Daniel
Lerner, Hans-Wolfram
Büttner, Dominik
Bolte, Michael
author_sort Franz, Daniel
collection PubMed
description The title compound, [Li(4)O(4)(C(12)H(8)BO)(4)(C(4)H(10)O)(4)], features a Li(4)O(4) cube. Each Li atom in the cube is additionally coordinated by a diethyl ether mol­ecule and each O atom in the cube carries a 9-oxa-10-boraanthracene residue. The crystal studied was a non-merohedral twin [twin law (-1 0 0 / 0 0 1 / 0 1 0); the contribution of the major twin component refined to 0.553 (3)] emulating apparent tetra­gonal symmetry, whereas the actual crystal system is just ortho­rhom­bic.
format Online
Article
Text
id pubmed-3246952
institution National Center for Biotechnology Information
language English
publishDate 2011
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32469522012-01-04 Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium] Franz, Daniel Lerner, Hans-Wolfram Büttner, Dominik Bolte, Michael Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers The title compound, [Li(4)O(4)(C(12)H(8)BO)(4)(C(4)H(10)O)(4)], features a Li(4)O(4) cube. Each Li atom in the cube is additionally coordinated by a diethyl ether mol­ecule and each O atom in the cube carries a 9-oxa-10-boraanthracene residue. The crystal studied was a non-merohedral twin [twin law (-1 0 0 / 0 0 1 / 0 1 0); the contribution of the major twin component refined to 0.553 (3)] emulating apparent tetra­gonal symmetry, whereas the actual crystal system is just ortho­rhom­bic. International Union of Crystallography 2011-10-12 /pmc/articles/PMC3246952/ /pubmed/22219772 http://dx.doi.org/10.1107/S1600536811041201 Text en © Franz et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Metal-Organic Papers
Franz, Daniel
Lerner, Hans-Wolfram
Büttner, Dominik
Bolte, Michael
Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
title Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
title_full Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
title_fullStr Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
title_full_unstemmed Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
title_short Tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
title_sort tetrakis(μ(3)-9-oxa-10-boraanthracen-10-olato)tetrakis[(diethyl ether)lithium]
topic Metal-Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3246952/
https://www.ncbi.nlm.nih.gov/pubmed/22219772
http://dx.doi.org/10.1107/S1600536811041201
work_keys_str_mv AT franzdaniel tetrakism39oxa10boraanthracen10olatotetrakisdiethyletherlithium
AT lernerhanswolfram tetrakism39oxa10boraanthracen10olatotetrakisdiethyletherlithium
AT buttnerdominik tetrakism39oxa10boraanthracen10olatotetrakisdiethyletherlithium
AT boltemichael tetrakism39oxa10boraanthracen10olatotetrakisdiethyletherlithium