(E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate

The title compound, C(35)H(35)NO(2)·CH(4)O, was obtained by the reaction of rac-2-amino-2-hy­droxy-1,1-binaphthyl and 3,5-di-tert-butyl-2-hy­droxy­benzaldehyde in absolute methanol. In the Schiff base mol­ecule, the two naphthyl bicycles are twisted by 71.15 (5)°. One hy­droxy group is involved in i...

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Detalles Bibliográficos
Autores principales: He, Dian, Li, Chong, Wang, Xiaohong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247328/
https://www.ncbi.nlm.nih.gov/pubmed/22219946
http://dx.doi.org/10.1107/S1600536811040116
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author He, Dian
Li, Chong
Wang, Xiaohong
author_facet He, Dian
Li, Chong
Wang, Xiaohong
author_sort He, Dian
collection PubMed
description The title compound, C(35)H(35)NO(2)·CH(4)O, was obtained by the reaction of rac-2-amino-2-hy­droxy-1,1-binaphthyl and 3,5-di-tert-butyl-2-hy­droxy­benzaldehyde in absolute methanol. In the Schiff base mol­ecule, the two naphthyl bicycles are twisted by 71.15 (5)°. One hy­droxy group is involved in intra­molecular O—H⋯N hydrogen bond, while the methanol solvent mol­ecule is linked to another hy­droxy group via an inter­molecular O—H⋯O hydrogen bond.
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spelling pubmed-32473282012-01-04 (E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate He, Dian Li, Chong Wang, Xiaohong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(35)H(35)NO(2)·CH(4)O, was obtained by the reaction of rac-2-amino-2-hy­droxy-1,1-binaphthyl and 3,5-di-tert-butyl-2-hy­droxy­benzaldehyde in absolute methanol. In the Schiff base mol­ecule, the two naphthyl bicycles are twisted by 71.15 (5)°. One hy­droxy group is involved in intra­molecular O—H⋯N hydrogen bond, while the methanol solvent mol­ecule is linked to another hy­droxy group via an inter­molecular O—H⋯O hydrogen bond. International Union of Crystallography 2011-10-12 /pmc/articles/PMC3247328/ /pubmed/22219946 http://dx.doi.org/10.1107/S1600536811040116 Text en © He et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
He, Dian
Li, Chong
Wang, Xiaohong
(E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
title (E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
title_full (E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
title_fullStr (E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
title_full_unstemmed (E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
title_short (E)-2′-[(3,5-Di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
title_sort (e)-2′-[(3,5-di-tert-butyl-2-hy­droxy­benzyl­idene)amino]-1,1′-binaphthalen-2-ol methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247328/
https://www.ncbi.nlm.nih.gov/pubmed/22219946
http://dx.doi.org/10.1107/S1600536811040116
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AT wangxiaohong e235ditertbutyl2hydroxybenzylideneamino11binaphthalen2olmethanolmonosolvate

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