1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one

The title mol­ecule, C(17)H(25)N(3)O(3), is built up from fused six- and five-membered rings linked to a –C(10)H(21) chain. The fused-ring system is essentially planar, the largest deviation from the mean plane being 0.009 (2) Å. The chain is roughly perpendic­ular to this plane, making a dihedral a...

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Detalles Bibliográficos
Autores principales: Ouzidan, Younes, Kandri Rodi, Youssef, Essassi, El Mokhtar, Luis, Santiago V., Bolte, Michael, El Ammari, Lahcen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247349/
https://www.ncbi.nlm.nih.gov/pubmed/22219967
http://dx.doi.org/10.1107/S1600536811041389
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author Ouzidan, Younes
Kandri Rodi, Youssef
Essassi, El Mokhtar
Luis, Santiago V.
Bolte, Michael
El Ammari, Lahcen
author_facet Ouzidan, Younes
Kandri Rodi, Youssef
Essassi, El Mokhtar
Luis, Santiago V.
Bolte, Michael
El Ammari, Lahcen
author_sort Ouzidan, Younes
collection PubMed
description The title mol­ecule, C(17)H(25)N(3)O(3), is built up from fused six- and five-membered rings linked to a –C(10)H(21) chain. The fused-ring system is essentially planar, the largest deviation from the mean plane being 0.009 (2) Å. The chain is roughly perpendic­ular to this plane, making a dihedral angle of 79.5 (2)°. In the crystal, N—H⋯O hydrogen bonds build infinite chains along [010]. There are channels in the structure containing disordered hexane. The contribution of this solvent to the scattering power was suppressed using the SQUEEZE option in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148–155].
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spelling pubmed-32473492012-01-04 1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one Ouzidan, Younes Kandri Rodi, Youssef Essassi, El Mokhtar Luis, Santiago V. Bolte, Michael El Ammari, Lahcen Acta Crystallogr Sect E Struct Rep Online Organic Papers The title mol­ecule, C(17)H(25)N(3)O(3), is built up from fused six- and five-membered rings linked to a –C(10)H(21) chain. The fused-ring system is essentially planar, the largest deviation from the mean plane being 0.009 (2) Å. The chain is roughly perpendic­ular to this plane, making a dihedral angle of 79.5 (2)°. In the crystal, N—H⋯O hydrogen bonds build infinite chains along [010]. There are channels in the structure containing disordered hexane. The contribution of this solvent to the scattering power was suppressed using the SQUEEZE option in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148–155]. International Union of Crystallography 2011-10-12 /pmc/articles/PMC3247349/ /pubmed/22219967 http://dx.doi.org/10.1107/S1600536811041389 Text en © Ouzidan et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ouzidan, Younes
Kandri Rodi, Youssef
Essassi, El Mokhtar
Luis, Santiago V.
Bolte, Michael
El Ammari, Lahcen
1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one
title 1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one
title_full 1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one
title_fullStr 1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one
title_full_unstemmed 1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one
title_short 1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one
title_sort 1-decyl-6-nitro-1h-benzimidazol-2(3h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247349/
https://www.ncbi.nlm.nih.gov/pubmed/22219967
http://dx.doi.org/10.1107/S1600536811041389
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