2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate

The title compound, C(11)H(11)N(3)O(2)·H(2)O, was obtained by the reaction of 2-acetyl­phenol with cyano­acetohydrazide in methanol. The asymmetric unit contains two hydrazone mol­ecules and two water mol­ecules of crystallization. There is an intra­molecular O—H⋯N hydrogen bond in each hydrazone mo...

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Detalles Bibliográficos
Autores principales: Li, Hongbo, Chen, Peng, You, Zhonglu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247401/
https://www.ncbi.nlm.nih.gov/pubmed/22220019
http://dx.doi.org/10.1107/S1600536811042565
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author Li, Hongbo
Chen, Peng
You, Zhonglu
author_facet Li, Hongbo
Chen, Peng
You, Zhonglu
author_sort Li, Hongbo
collection PubMed
description The title compound, C(11)H(11)N(3)O(2)·H(2)O, was obtained by the reaction of 2-acetyl­phenol with cyano­acetohydrazide in methanol. The asymmetric unit contains two hydrazone mol­ecules and two water mol­ecules of crystallization. There is an intra­molecular O—H⋯N hydrogen bond in each hydrazone mol­ecule. The crystal structure is stabilized by inter­molecular N—H⋯O, O—H⋯O and O—H⋯N hydrogen bonds.
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spelling pubmed-32474012012-01-04 2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate Li, Hongbo Chen, Peng You, Zhonglu Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(11)N(3)O(2)·H(2)O, was obtained by the reaction of 2-acetyl­phenol with cyano­acetohydrazide in methanol. The asymmetric unit contains two hydrazone mol­ecules and two water mol­ecules of crystallization. There is an intra­molecular O—H⋯N hydrogen bond in each hydrazone mol­ecule. The crystal structure is stabilized by inter­molecular N—H⋯O, O—H⋯O and O—H⋯N hydrogen bonds. International Union of Crystallography 2011-10-22 /pmc/articles/PMC3247401/ /pubmed/22220019 http://dx.doi.org/10.1107/S1600536811042565 Text en © Li et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Hongbo
Chen, Peng
You, Zhonglu
2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
title 2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
title_full 2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
title_fullStr 2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
title_full_unstemmed 2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
title_short 2-Cyano-N′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
title_sort 2-cyano-n′-[1-(2-hy­droxy­phen­yl)ethyl­idene]acetohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247401/
https://www.ncbi.nlm.nih.gov/pubmed/22220019
http://dx.doi.org/10.1107/S1600536811042565
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AT chenpeng 2cyanon12hydroxyphenylethylideneacetohydrazidemonohydrate
AT youzhonglu 2cyanon12hydroxyphenylethylideneacetohydrazidemonohydrate

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