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N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide
In the title compound, C(24)H(28)N(2)O(4)S(2), the dihedral angles between the central benzene ring and the pendant rings are 77.44 (11) and 79.23 (10)°, and the dihedral angle between the pendant rings is 23.31 (12)°. Both sulfonamide groups project to the same side of the central benzene ring and...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247432/ https://www.ncbi.nlm.nih.gov/pubmed/22220050 http://dx.doi.org/10.1107/S1600536811040700 |
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author | Ejaz, Khan, Islam Ullah Ahmad, Hira Harrison, William T. A. Sheikh, Tahir Ali |
author_facet | Ejaz, Khan, Islam Ullah Ahmad, Hira Harrison, William T. A. Sheikh, Tahir Ali |
author_sort | Ejaz, |
collection | PubMed |
description | In the title compound, C(24)H(28)N(2)O(4)S(2), the dihedral angles between the central benzene ring and the pendant rings are 77.44 (11) and 79.23 (10)°, and the dihedral angle between the pendant rings is 23.31 (12)°. Both sulfonamide groups project to the same side of the central benzene ring and the molecule has approximate non-crystallographic mirror symmetry. One of the ethyl side chains is disordered over two sets of sites in a 0.526 (14):0.474 (14) ratio. In the crystal, inversion dimers linked by pairs of weak C—H⋯O interactions occur, generating R (2) (2)(28) loops. |
format | Online Article Text |
id | pubmed-3247432 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2011 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-32474322012-01-04 N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide Ejaz, Khan, Islam Ullah Ahmad, Hira Harrison, William T. A. Sheikh, Tahir Ali Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(24)H(28)N(2)O(4)S(2), the dihedral angles between the central benzene ring and the pendant rings are 77.44 (11) and 79.23 (10)°, and the dihedral angle between the pendant rings is 23.31 (12)°. Both sulfonamide groups project to the same side of the central benzene ring and the molecule has approximate non-crystallographic mirror symmetry. One of the ethyl side chains is disordered over two sets of sites in a 0.526 (14):0.474 (14) ratio. In the crystal, inversion dimers linked by pairs of weak C—H⋯O interactions occur, generating R (2) (2)(28) loops. International Union of Crystallography 2011-10-29 /pmc/articles/PMC3247432/ /pubmed/22220050 http://dx.doi.org/10.1107/S1600536811040700 Text en © Ejaz et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Ejaz, Khan, Islam Ullah Ahmad, Hira Harrison, William T. A. Sheikh, Tahir Ali N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
title |
N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
title_full |
N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
title_fullStr |
N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
title_full_unstemmed |
N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
title_short |
N,N′-Diethyl-N,N′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
title_sort | n,n′-diethyl-n,n′-[1,3-phenylenebis(methylene)]dibenzenesulfonamide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247432/ https://www.ncbi.nlm.nih.gov/pubmed/22220050 http://dx.doi.org/10.1107/S1600536811040700 |
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