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N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide

In the title compound, C(24)H(28)N(2)O(4)S(2), the dihedral angles between the central benzene ring and the pendant rings are 77.44 (11) and 79.23 (10)°, and the dihedral angle between the pendant rings is 23.31 (12)°. Both sulfonamide groups project to the same side of the central benzene ring and...

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Autores principales: Ejaz, Khan, Islam Ullah, Ahmad, Hira, Harrison, William T. A., Sheikh, Tahir Ali
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247432/
https://www.ncbi.nlm.nih.gov/pubmed/22220050
http://dx.doi.org/10.1107/S1600536811040700
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author Ejaz,
Khan, Islam Ullah
Ahmad, Hira
Harrison, William T. A.
Sheikh, Tahir Ali
author_facet Ejaz,
Khan, Islam Ullah
Ahmad, Hira
Harrison, William T. A.
Sheikh, Tahir Ali
author_sort Ejaz,
collection PubMed
description In the title compound, C(24)H(28)N(2)O(4)S(2), the dihedral angles between the central benzene ring and the pendant rings are 77.44 (11) and 79.23 (10)°, and the dihedral angle between the pendant rings is 23.31 (12)°. Both sulfonamide groups project to the same side of the central benzene ring and the mol­ecule has approximate non-crystallographic mirror symmetry. One of the ethyl side chains is disordered over two sets of sites in a 0.526 (14):0.474 (14) ratio. In the crystal, inversion dimers linked by pairs of weak C—H⋯O inter­actions occur, generating R (2) (2)(28) loops.
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spelling pubmed-32474322012-01-04 N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide Ejaz, Khan, Islam Ullah Ahmad, Hira Harrison, William T. A. Sheikh, Tahir Ali Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(24)H(28)N(2)O(4)S(2), the dihedral angles between the central benzene ring and the pendant rings are 77.44 (11) and 79.23 (10)°, and the dihedral angle between the pendant rings is 23.31 (12)°. Both sulfonamide groups project to the same side of the central benzene ring and the mol­ecule has approximate non-crystallographic mirror symmetry. One of the ethyl side chains is disordered over two sets of sites in a 0.526 (14):0.474 (14) ratio. In the crystal, inversion dimers linked by pairs of weak C—H⋯O inter­actions occur, generating R (2) (2)(28) loops. International Union of Crystallography 2011-10-29 /pmc/articles/PMC3247432/ /pubmed/22220050 http://dx.doi.org/10.1107/S1600536811040700 Text en © Ejaz et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ejaz,
Khan, Islam Ullah
Ahmad, Hira
Harrison, William T. A.
Sheikh, Tahir Ali
N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
title N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
title_full N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
title_fullStr N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
title_full_unstemmed N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
title_short N,N′-Diethyl-N,N′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
title_sort n,n′-diethyl-n,n′-[1,3-phenylene­bis(methyl­ene)]dibenzene­sulfonamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247432/
https://www.ncbi.nlm.nih.gov/pubmed/22220050
http://dx.doi.org/10.1107/S1600536811040700
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