4-Chloro-N′-(2-hy­droxy-4-meth­oxy­benzyl­idene)benzohydrazide methanol monosolvate

The title compound, C(15)H(13)ClN(2)O(3)·CH(3)OH, was synthesized by the condensation reaction of 2-hy­droxy-4-meth­oxy­benzaldehyde with 4-chloro­benzohydrazide in methanol. The Schiff base mol­ecule displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between th...

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Detalles Bibliográficos
Autores principales: Zhi, Feng, Wang, Rong, Zhang, Yi, Wang, Qiang, Yang, Yi-Lin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3247565/
https://www.ncbi.nlm.nih.gov/pubmed/22219870
http://dx.doi.org/10.1107/S1600536811039778
Descripción
Sumario:The title compound, C(15)H(13)ClN(2)O(3)·CH(3)OH, was synthesized by the condensation reaction of 2-hy­droxy-4-meth­oxy­benzaldehyde with 4-chloro­benzohydrazide in methanol. The Schiff base mol­ecule displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the two benzene rings is 5.3 (2)°. In the crystal, mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen-bond inter­actions into chains running parallel to the a axis. An intra­molecular O—H⋯N hydrogen bond is observed.

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