Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)

In the pyrimidine mol­ecule of the title compound, C(9)H(7)N(3)·C(9)H(6)O(6), the pyridine ring is oriented at 33.26 (11)° with respect to the pyrimidine ring. In the benzene-1,3,5-tricarb­oxy­lic acid mol­ecule, the three carb­oxy groups are twisted by 7.92 (9), 8.68 (10) and 17.07 (10)° relative t...

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Detalles Bibliográficos
Autores principales: Jiang, Yan-Ke, Hou, Gui-Ge
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254286/
https://www.ncbi.nlm.nih.gov/pubmed/22259560
http://dx.doi.org/10.1107/S1600536811051075
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author Jiang, Yan-Ke
Hou, Gui-Ge
author_facet Jiang, Yan-Ke
Hou, Gui-Ge
author_sort Jiang, Yan-Ke
collection PubMed
description In the pyrimidine mol­ecule of the title compound, C(9)H(7)N(3)·C(9)H(6)O(6), the pyridine ring is oriented at 33.26 (11)° with respect to the pyrimidine ring. In the benzene-1,3,5-tricarb­oxy­lic acid mol­ecule, the three carb­oxy groups are twisted by 7.92 (9), 8.68 (10) and 17.07 (10)° relative to the benzene ring. Classical O—H⋯N and O—H⋯O hydrogen bonds and weak C—H⋯O and C—H⋯N hydrogen bonds occur in the crystal structure.
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spelling pubmed-32542862012-01-18 Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1) Jiang, Yan-Ke Hou, Gui-Ge Acta Crystallogr Sect E Struct Rep Online Organic Papers In the pyrimidine mol­ecule of the title compound, C(9)H(7)N(3)·C(9)H(6)O(6), the pyridine ring is oriented at 33.26 (11)° with respect to the pyrimidine ring. In the benzene-1,3,5-tricarb­oxy­lic acid mol­ecule, the three carb­oxy groups are twisted by 7.92 (9), 8.68 (10) and 17.07 (10)° relative to the benzene ring. Classical O—H⋯N and O—H⋯O hydrogen bonds and weak C—H⋯O and C—H⋯N hydrogen bonds occur in the crystal structure. International Union of Crystallography 2011-12-03 /pmc/articles/PMC3254286/ /pubmed/22259560 http://dx.doi.org/10.1107/S1600536811051075 Text en © Jiang and Hou 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jiang, Yan-Ke
Hou, Gui-Ge
Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
title Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
title_full Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
title_fullStr Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
title_full_unstemmed Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
title_short Benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
title_sort benzene-1,3,5-tricarb­oxy­lic acid–5-(4-pyrid­yl)pyrimidine (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254286/
https://www.ncbi.nlm.nih.gov/pubmed/22259560
http://dx.doi.org/10.1107/S1600536811051075
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