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(3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate

In the title compound, C(13)H(19)ClN(3)O(3) (+)·ClO(4) (−), the 3-(di­meth­yl­ammonio)­propyl group of the cation is disordered over two sets of sites with occupancies 0.772 (6) and 0.228 (6). The cations are joined by pairs of N—H⋯O hydrogen bonds into centrosymmetric dimers and these dimers are as...

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Detalles Bibliográficos
Autores principales: Yue, Xi-Teng, Li, Xiao-Wen, Wu, Zhi-Yong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254288/
https://www.ncbi.nlm.nih.gov/pubmed/22259579
http://dx.doi.org/10.1107/S1600536811050653
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author Yue, Xi-Teng
Li, Xiao-Wen
Wu, Zhi-Yong
author_facet Yue, Xi-Teng
Li, Xiao-Wen
Wu, Zhi-Yong
author_sort Yue, Xi-Teng
collection PubMed
description In the title compound, C(13)H(19)ClN(3)O(3) (+)·ClO(4) (−), the 3-(di­meth­yl­ammonio)­propyl group of the cation is disordered over two sets of sites with occupancies 0.772 (6) and 0.228 (6). The cations are joined by pairs of N—H⋯O hydrogen bonds into centrosymmetric dimers and these dimers are assembled into chains along the a-axis direction, also through N—H⋯O hydrogen bonds. The perchlorate anions are linked to the hy­droxy groups of the cations by O—H⋯O hydrogen bonds. The positively charged ammonium groups and the anions give rise to folded layers parallel to the ab plane.
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spelling pubmed-32542882012-01-18 (3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate Yue, Xi-Teng Li, Xiao-Wen Wu, Zhi-Yong Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(19)ClN(3)O(3) (+)·ClO(4) (−), the 3-(di­meth­yl­ammonio)­propyl group of the cation is disordered over two sets of sites with occupancies 0.772 (6) and 0.228 (6). The cations are joined by pairs of N—H⋯O hydrogen bonds into centrosymmetric dimers and these dimers are assembled into chains along the a-axis direction, also through N—H⋯O hydrogen bonds. The perchlorate anions are linked to the hy­droxy groups of the cations by O—H⋯O hydrogen bonds. The positively charged ammonium groups and the anions give rise to folded layers parallel to the ab plane. International Union of Crystallography 2011-12-03 /pmc/articles/PMC3254288/ /pubmed/22259579 http://dx.doi.org/10.1107/S1600536811050653 Text en © Yue et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yue, Xi-Teng
Li, Xiao-Wen
Wu, Zhi-Yong
(3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
title (3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
title_full (3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
title_fullStr (3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
title_full_unstemmed (3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
title_short (3-{[N-(5-Chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
title_sort (3-{[n-(5-chloro-2-hy­droxy­phen­yl)oxamo­yl]amino}­prop­yl)dimethyl­aza­nium perchlorate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254288/
https://www.ncbi.nlm.nih.gov/pubmed/22259579
http://dx.doi.org/10.1107/S1600536811050653
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