(1H-Benzimidazol-2-yl)methanaminium perchlorate–18-crown-6–water (1/1/1)

The crystal structure of the title compound C(8)H(10)N(3) (+)·ClO(4) (−)·C(12)H(24)O(6)·H(2)O, consists of an organic (1H-benzimidazol-2-yl)methanaminium cation, an inorganic ClO(4) (−) anion, one 18-crown-6 mol­ecule and one water mol­ecule. In the crystal, the cations and 18-crown-6 mol­ecules are...

Descripción completa

Detalles Bibliográficos
Autor principal: Sun, Su-Wen
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254365/
https://www.ncbi.nlm.nih.gov/pubmed/22259530
http://dx.doi.org/10.1107/S1600536811050665
Descripción
Sumario:The crystal structure of the title compound C(8)H(10)N(3) (+)·ClO(4) (−)·C(12)H(24)O(6)·H(2)O, consists of an organic (1H-benzimidazol-2-yl)methanaminium cation, an inorganic ClO(4) (−) anion, one 18-crown-6 mol­ecule and one water mol­ecule. In the crystal, the cations and 18-crown-6 mol­ecules are linked by N—H⋯O hydrogen bonds. The crystal packing is stabilized by inter­molecular O—H⋯O, O—H⋯N and O—H⋯Cl hydrogen bonds between anions and the water mol­ecules. One 18-crown-6 C atom and a perchlorate O atom are disordered; both have an occupancy factor ratio of 0.60 (2) and 0.40 (2).

Ejemplares similares