4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate

In the title compound, C(14)H(12)ClNO(3)S·H(2)O, the dihedral angle between the sulfonyl and benzoyl benzene rings is 84.4 (2)°. In the crystal, every water mol­ecule forms four hydrogen bonds with three different mol­ecules of 4-chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide. One of the water H at...

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Autores principales: Suchetan, P. A., Foro, Sabine, Gowda, B. Thimme, Prakash, M. Shet
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254406/
https://www.ncbi.nlm.nih.gov/pubmed/22259549
http://dx.doi.org/10.1107/S1600536811051932
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author Suchetan, P. A.
Foro, Sabine
Gowda, B. Thimme
Prakash, M. Shet
author_facet Suchetan, P. A.
Foro, Sabine
Gowda, B. Thimme
Prakash, M. Shet
author_sort Suchetan, P. A.
collection PubMed
description In the title compound, C(14)H(12)ClNO(3)S·H(2)O, the dihedral angle between the sulfonyl and benzoyl benzene rings is 84.4 (2)°. In the crystal, every water mol­ecule forms four hydrogen bonds with three different mol­ecules of 4-chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide. One of the water H atoms forms a bifurcated hydrogen bond with both the sulfonyl and the carbonyl O atoms of the same mol­ecule. Mol­ecules are linked into layers in the ab plane through N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-32544062012-01-18 4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate Suchetan, P. A. Foro, Sabine Gowda, B. Thimme Prakash, M. Shet Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(12)ClNO(3)S·H(2)O, the dihedral angle between the sulfonyl and benzoyl benzene rings is 84.4 (2)°. In the crystal, every water mol­ecule forms four hydrogen bonds with three different mol­ecules of 4-chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide. One of the water H atoms forms a bifurcated hydrogen bond with both the sulfonyl and the carbonyl O atoms of the same mol­ecule. Mol­ecules are linked into layers in the ab plane through N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2011-12-07 /pmc/articles/PMC3254406/ /pubmed/22259549 http://dx.doi.org/10.1107/S1600536811051932 Text en © Suchetan et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Suchetan, P. A.
Foro, Sabine
Gowda, B. Thimme
Prakash, M. Shet
4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
title 4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
title_full 4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
title_fullStr 4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
title_full_unstemmed 4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
title_short 4-Chloro-N-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
title_sort 4-chloro-n-(3-methyl­benzo­yl)benzene­sulfonamide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254406/
https://www.ncbi.nlm.nih.gov/pubmed/22259549
http://dx.doi.org/10.1107/S1600536811051932
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AT gowdabthimme 4chloron3methylbenzoylbenzenesulfonamidemonohydrate
AT prakashmshet 4chloron3methylbenzoylbenzenesulfonamidemonohydrate

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