(2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone

The title compound, C(17)H(13)ClN(2)OS, crystallizes with three independent mol­ecules (A, B and C) in the asymmetric unit which differ slightly in their conformations. In mol­ecule A, the thiazole ring makes dihedral angles of 27.44 (14) and 66.05 (6)° with the phenyl and chloro­benzene rings. In m...

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Detalles Bibliográficos
Autores principales: Liu, Jing-Jing, Zheng, Ren-Lin, Yang, Sheng-Yong, Xie, Yong-Mei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254502/
https://www.ncbi.nlm.nih.gov/pubmed/22259446
http://dx.doi.org/10.1107/S1600536811053463
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author Liu, Jing-Jing
Zheng, Ren-Lin
Yang, Sheng-Yong
Xie, Yong-Mei
author_facet Liu, Jing-Jing
Zheng, Ren-Lin
Yang, Sheng-Yong
Xie, Yong-Mei
author_sort Liu, Jing-Jing
collection PubMed
description The title compound, C(17)H(13)ClN(2)OS, crystallizes with three independent mol­ecules (A, B and C) in the asymmetric unit which differ slightly in their conformations. In mol­ecule A, the thiazole ring makes dihedral angles of 27.44 (14) and 66.05 (6)° with the phenyl and chloro­benzene rings. In mol­ecule B, the respective angles are 29.09 (10) and 47.63 (9)°, while values of 25.67 (11) and 51.01 (7)° are observed in mol­ecule C. In the crystal, N—H⋯N and N—H⋯O hydrogen bonds generate a three-dimensional network structure.
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spelling pubmed-32545022012-01-18 (2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone Liu, Jing-Jing Zheng, Ren-Lin Yang, Sheng-Yong Xie, Yong-Mei Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(13)ClN(2)OS, crystallizes with three independent mol­ecules (A, B and C) in the asymmetric unit which differ slightly in their conformations. In mol­ecule A, the thiazole ring makes dihedral angles of 27.44 (14) and 66.05 (6)° with the phenyl and chloro­benzene rings. In mol­ecule B, the respective angles are 29.09 (10) and 47.63 (9)°, while values of 25.67 (11) and 51.01 (7)° are observed in mol­ecule C. In the crystal, N—H⋯N and N—H⋯O hydrogen bonds generate a three-dimensional network structure. International Union of Crystallography 2011-12-17 /pmc/articles/PMC3254502/ /pubmed/22259446 http://dx.doi.org/10.1107/S1600536811053463 Text en © Liu et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Jing-Jing
Zheng, Ren-Lin
Yang, Sheng-Yong
Xie, Yong-Mei
(2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
title (2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
title_full (2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
title_fullStr (2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
title_full_unstemmed (2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
title_short (2-Anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
title_sort (2-anilino-4-methyl­thia­zol-5-yl)(4-chloro­phen­yl)methanone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254502/
https://www.ncbi.nlm.nih.gov/pubmed/22259446
http://dx.doi.org/10.1107/S1600536811053463
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AT zhengrenlin 2anilino4methylthiazol5yl4chlorophenylmethanone
AT yangshengyong 2anilino4methylthiazol5yl4chlorophenylmethanone
AT xieyongmei 2anilino4methylthiazol5yl4chlorophenylmethanone

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