3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one

The asymmetric unit of the title compound, C(18)H(18)N(2)O(2), contains three independent mol­ecules. In each, the seven-membered diazepine ring adopts a boat conformation with the hy­droxy-substituted C atom at the prow and fused-ring C atoms at the stern. In the crystal, the mol­ecules are linked...

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Detalles Bibliográficos
Autores principales: Rida, Mohamed, Mamari, Khalil, Essassi, El Mokhtar, Ng, Seik Weng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254569/
https://www.ncbi.nlm.nih.gov/pubmed/22259519
http://dx.doi.org/10.1107/S1600536811054456
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author Rida, Mohamed
Mamari, Khalil
Essassi, El Mokhtar
Ng, Seik Weng
author_facet Rida, Mohamed
Mamari, Khalil
Essassi, El Mokhtar
Ng, Seik Weng
author_sort Rida, Mohamed
collection PubMed
description The asymmetric unit of the title compound, C(18)H(18)N(2)O(2), contains three independent mol­ecules. In each, the seven-membered diazepine ring adopts a boat conformation with the hy­droxy-substituted C atom at the prow and fused-ring C atoms at the stern. In the crystal, the mol­ecules are linked by O—H⋯O and N—H⋯O hydrogen bonds. The allyl group of one mol­ecule is equally disordered over two positions.
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spelling pubmed-32545692012-01-18 3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one Rida, Mohamed Mamari, Khalil Essassi, El Mokhtar Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(18)H(18)N(2)O(2), contains three independent mol­ecules. In each, the seven-membered diazepine ring adopts a boat conformation with the hy­droxy-substituted C atom at the prow and fused-ring C atoms at the stern. In the crystal, the mol­ecules are linked by O—H⋯O and N—H⋯O hydrogen bonds. The allyl group of one mol­ecule is equally disordered over two positions. International Union of Crystallography 2011-12-23 /pmc/articles/PMC3254569/ /pubmed/22259519 http://dx.doi.org/10.1107/S1600536811054456 Text en © Rida et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rida, Mohamed
Mamari, Khalil
Essassi, El Mokhtar
Ng, Seik Weng
3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one
title 3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one
title_full 3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one
title_fullStr 3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one
title_full_unstemmed 3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one
title_short 3-Hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1H-1,5-benzodiazepin-2-one
title_sort 3-hy­droxy-4-phenyl-1-(prop-2-en-1-yl)-2,3,4,5-tetra­hydro-1h-1,5-benzodiazepin-2-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3254569/
https://www.ncbi.nlm.nih.gov/pubmed/22259519
http://dx.doi.org/10.1107/S1600536811054456
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