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Three-dimensional diffraction mapping by tuning the X-ray energy

Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by...

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Autores principales: Cornelius, T. W., Carbone, D., Jacques, V. L. R., Schülli, T. U., Metzger, T. H.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2011
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3268694/
https://www.ncbi.nlm.nih.gov/pubmed/21525649
http://dx.doi.org/10.1107/S0909049511003190
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author Cornelius, T. W.
Carbone, D.
Jacques, V. L. R.
Schülli, T. U.
Metzger, T. H.
author_facet Cornelius, T. W.
Carbone, D.
Jacques, V. L. R.
Schülli, T. U.
Metzger, T. H.
author_sort Cornelius, T. W.
collection PubMed
description Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by an ordinary rocking-curve scan. The energy-tuning approach circumvents both the comparatively large sphere of confusion of diffractometers compared with nanostructures and vibrations induced by motors. Thus, this method offers new possibilities for novel combinations of three-dimensional micro- and nano-focused X-ray diffraction with complex in situ sample environments such as scanning probe microscopes.
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spelling pubmed-32686942012-01-31 Three-dimensional diffraction mapping by tuning the X-ray energy Cornelius, T. W. Carbone, D. Jacques, V. L. R. Schülli, T. U. Metzger, T. H. J Synchrotron Radiat Research Papers Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by an ordinary rocking-curve scan. The energy-tuning approach circumvents both the comparatively large sphere of confusion of diffractometers compared with nanostructures and vibrations induced by motors. Thus, this method offers new possibilities for novel combinations of three-dimensional micro- and nano-focused X-ray diffraction with complex in situ sample environments such as scanning probe microscopes. International Union of Crystallography 2011-05-01 2011-03-15 /pmc/articles/PMC3268694/ /pubmed/21525649 http://dx.doi.org/10.1107/S0909049511003190 Text en © T. W. Cornelius et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Cornelius, T. W.
Carbone, D.
Jacques, V. L. R.
Schülli, T. U.
Metzger, T. H.
Three-dimensional diffraction mapping by tuning the X-ray energy
title Three-dimensional diffraction mapping by tuning the X-ray energy
title_full Three-dimensional diffraction mapping by tuning the X-ray energy
title_fullStr Three-dimensional diffraction mapping by tuning the X-ray energy
title_full_unstemmed Three-dimensional diffraction mapping by tuning the X-ray energy
title_short Three-dimensional diffraction mapping by tuning the X-ray energy
title_sort three-dimensional diffraction mapping by tuning the x-ray energy
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3268694/
https://www.ncbi.nlm.nih.gov/pubmed/21525649
http://dx.doi.org/10.1107/S0909049511003190
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